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Joining of SiC by tape-cast SiC-Al_2O_3-Y_2O_3 interlayer

机译:通过磁带铸造SiC-AL_2O_3-Y_2O_3中间层加入SIC

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SiC substrates were successfully bonded by tape-cast SiC-Al_2O_3-Y_2O_3 interlayers in the temperature range of 1800-1900 °C for 60 min at 15 MPa pressure in flowing Ar. Based on microstructure observations, we find that the a-SiC interlayers result in equiaxed microstructure at all joining temperatures while the tape-cast P-SiC leads to a microstructure varying from a mixed characteristic to an elongated one with joining temperature. The detailed image analysis suggests the close interlayer thickness, the quicker grain growth rate of P-SiC relative to a-SiC one and the good agreement between aspect ratio and morphology in all joints. Moreover, the SiC grains of interlayer near to interface develop preferentially from the external SiC grains of substrate, which is possibly related to the morphology difference between substrate and interlayer and the grain growth behaviors. Finally, the SiC joined with tapes exhibits an average bending strength over 359 MPa and usually fracture within SiC bases.
机译:通过在15MPa的流动的AR中以1800-1900℃的温度范围内的温度范围内通过胶束浇铸SiC-Al_2O_3-Y_2O_3中间层成功键合。基于微观结构观察,发现A-SiC夹层在所有接合温度下导致等式的微观结构,而胶带铸造P-SiC导致从混合特性与具有接合温度的细长α的微观结构变化。详细的图像分析表明,相对于A-SiC的P-SiC的更快的晶粒生长速率和所有关节中的纵横比和形态之间的良好一致性。此外,邻接界面附近的中间层的SiC晶粒优选地从基板的外部SiC晶粒进行,这可能与基材和中间层之间的形态学和晶粒生长行为有关。最后,连接磁带的SiC表现出超过359MPa的平均弯曲强度,并且通常在SiC基础内裂缝。

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