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Surface morphology and field emission of cubic boron nitride thin films

机译:立方硼氮化物薄膜的表面形态和场发射

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Field emission results from an on-going study of thin films of polycrystalline cubic boron nitride (cBN) are presented. Samples under study have been synthesized using the reduced-bias ion-assisted sputtering technique [1], which enables the growth of 100% cubic phase up to 2μm in thickness. Si(100) substrates have been utilized for this experiment. Reflection High energy Electron Diffraction (RHEED) was used to characterize the surface morphology of the deposited films in situ; Scanning Electron Microscopy (SEM) and Atomic Force Microscopy (AFM) data of the BN thin films were obtained outside the growth environment. Fourier Transform Infrared Spectroscopy (FTIR) provided crystal phase and composition information of the boron nitride films. The field emission of the BN films grown to various thicknesses was examined, using a customized parallel plate configuration at pressures of 10~(-8) Torr or lower. Conclusions based on the analysis of these emission results are offered with particular regard to the effects of the different morphology of the film surface, which consequently provides insight into the field emission characteristics of the cBN thin film itself.
机译:提出了一种现场排放来自多晶立方氮化硼(CBN)的薄膜的正在进行的研究。使用降偏离离子辅助溅射技术[1]合成正在研究的样品,这使得能够厚度为100%立方相的生长至2μm。 Si(100)基材已用于该实验。反射高能量电子衍射(RHEED)用于表征沉积薄膜的表面形态;扫描电子显微镜(SEM)和原子力显微镜(AFM)的BN薄膜的数据在生长环境之外获得。傅里叶变换红外光谱(FTIR)提供了氮化硼膜的晶相和组成信息。检查生长到各种厚度的BN膜的场发射,在10〜(8)托尔或更低的压力下使用定制的平行板构造。基于对这些排放结果的分析的结论特别考虑了薄膜表面的不同形貌的影响,从而提供了进入CBN薄膜本身的场发射特性的洞察。

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