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THERMAL CONDUCTANCE OF BI-MATERIAL AFM CANTILEVERS

机译:双材料AFM悬臂梁的导热系数

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摘要

In this letter, based on the beam theory and the thermal analysis of a bi-material cantilever, we demonstrate that the effective thermal conductance of the cantilever and the temperature at the tip of the cantilever can be determined by measuring the bending of the cantilever in response to two different thermal inputs: power absorbed at the tip and ambient temperature.The bi-material cantilevers were first introduced as a calorimeter to measure the heat generated in chemical reactions.[1] The same device was demonstrated to be sensitive enough to measure power as small as 100 pW or energy of 150 fJ in photothermal measurements. [2] They were also used as IR detectors [3,4,5] or as scanning thermal imaging probes.[6] Although the bi-material cantilevers are often used as temperature or heat flux sensors based on the beam bending due to the unequal thermal expansion of the two materials, the exact temperature at the tip of the cantilever is usually unknown. Directly measuring the temperature is difficult due to the small geometry of the cantilever structure. To find out the temperature of the cantilever, one should obtain the thermal conductance of the cantilever. However, since the thermal properties of twolayers of the cantilever are dependent on their thickness, one cannot rely on theoretical calculation. In this letter, we develop a technique to determine the thermal conductance of the cantilever by measuring the bending of the cantilever in response to the variations of the absorbed power at the tip and the ambient temperature.A triangular silicon nitride cantilever coaled with 70 nm gold film is used in the current experiment. As shown in Fig.1 (a), a semiconductor laser beam is focused on the tip of the cantilever and reflected onto a position sensing detector (PSD). The deflection of the reflected laser beam spot on the PSD is used as a measure of the deflection of the cantilever. A part of the laser power is absorbed by the cantilever and thus creates a temperature rise at the end of the cantilever. The output of the PSD is converted into an X or Y signal corresponding to the position of the laser spot on the PSD and a sum signal proportional to the incident laser power.
机译:在这封信中,基于射线理论和双材料悬臂梁的热分析,我们证明了悬臂梁的有效热导率和悬臂梁尖端的温度可以通过测量悬臂梁的弯曲度来确定。对两个不同热输入的响应:尖端吸收的功率和环境温度。 首先引入双材料悬臂作为量热仪,以测量化学反应中产生的热量。[1]事实证明,同一装置足够灵敏,可以在光热测量中测量小至100 pW的功率或150 fJ的能量。 [2]它们还用作红外探测器[3,4,5]或扫描热成像探头。[6]尽管由于两种材料的热膨胀不相等,基于材料弯曲的双材料悬臂经常被用作温度或热通量传感器,但悬臂尖端的确切温度通常是未知的。由于悬臂结构的几何形状小,因此直接测量温度是困难的。为了找出悬臂的温度,应该获得悬臂的热导率。但是,由于两种 悬臂的各层取决于其厚度,不能依靠理论计算。在这封信中,我们开发了一种技术,该技术通过测量悬臂的弯曲来确定悬臂的热导,以响应尖端吸收的功率和环境温度的变化。 在本实验中,使用了结合有70 nm金膜的三角形氮化硅悬臂。如图1(a)所示,半导体激光束聚焦在悬臂的尖端,并反射到位置检测器(PSD)上。 PSD上反射激光束光斑的偏转被用作悬臂偏转的量度。一部分激光功率被悬臂吸收,因此在悬臂末端产生温度升高。 PSD的输出被转换为与PSD上的激光光斑位置相对应的X或Y信号,以及与入射激光功率成正比的总和信号。

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