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Sand-blasting treatment as a way to improve the adhesion strength of hydroxyapatite coating on titanium implant

机译:喷砂处理作为提高钛植入羟基磷灰石涂层粘附强度的一种方法

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In the current study, the effect of corundum particle sizes (50 and 250-320 μm) used for sand-blasting on the structure, roughness, wettability, mechanical properties, and adhesion of radio frequency magnetron hydroxyapatite coating deposited on treated titanium substrate is studied. Morphology analysis revealed that pretreatment uniformly deforms the surface and induces the formation of pits, which size depends linearly on the grit size. The deposited coatings (Ca/P was in a range of 1.75-1.79) are homogeneous and repeat the relief of the substrate (mean roughness Ra is 1.9±0.1 (250-320 μm) and 0.8±0.1 μm (50 μm)). Texture coefficient calculations revealed the predominant (002) growth texture of hydroxyapatite coatings. The resistance of the coating to plastic deformation and the surface hardening were significantly higher for coatings formed on sand blasted with particle size of 50 μm. Scratch test have shown the significant improvement of wear resistance and lower friction coefficient of coatings for smoother samples. Dynamic contact angle measurements revealed the hydrophilic properties of the hydroxyapatite coating. Thus, sand-blasting of titanium with corundum powder having the size of 50 μm prior to the deposition of RF magnetron coating is recommended for the medical applications intended to improve the bonding between the substrate and coating.
机译:在本研究中,研究了用于在经处理的钛基材上沉积在处理过的钛基底上的结构,粗糙度,润湿性,机械性能和粘合射击射击射击的血液粒度(50和250-320μm)的影响。形态学分析显示,预处理均匀地变形表面并诱导凹坑的形成,该尺寸在砂砾尺寸上线性取决于线性。沉积的涂层(Ca / P在1.75-1.79的范围内)是均匀的,重复基材的浮雕(平均粗糙度Ra为1.9±0.1(250-320μm)和0.8±0.1μm(50μm))。纹理系数计算揭示了羟基磷灰石涂层的主要(002)生长纹理。对于在颗粒尺寸为50μm的沙子上形成的涂层上,涂层对塑料变形和表面硬化的电阻显着较高。划痕试验表明耐磨性的显着改善和涂层涂层的较低摩擦系数。动态接触角测量显示羟基磷灰石涂层的亲水性。因此,建议在沉积RF磁控涂层之前用浓度为50μm的核粉末喷砂,用于改善基板与涂层之间的粘合的医疗应用。

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