首页> 外文会议>International Symposium on Nanoporous Materials; 20050607-10; Niagara Falls(CA) >One-pot synthesis and characterization of high surface area perovskite-type BaTiO_3 with mesoporous texture
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One-pot synthesis and characterization of high surface area perovskite-type BaTiO_3 with mesoporous texture

机译:介孔结构高表面积钙钛矿型BaTiO_3的一锅合成及表征

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High surface area perovskite-type BaTiO_3 with mesoporous texture were prepared via hydrothermal and solvothermal method and then characterized by TEM, XRD and BET. The results revealed that samples synthesized by the different methods had high surface area of 52 and 61 m~2.g~(-1), respectively. The as-synthesized sample via hydrothermal method has better thermal stability. The catalytic performance of the samples was investigated by selective oxidation and dehydrogenation of benzyl alcohol, which indicated that the high surface area of BaTiO_3 could enhance the total conversion and the selectivity of benzylaldehyde.
机译:通过水热和溶剂热法制备了具有介孔结构的高表面积钙钛矿型BaTiO_3,然后用TEM,XRD和BET对其进行了表征。结果表明,用不同方法合成的样品的表面积分别为52和61 m〜2.g〜(-1)。通过水热法合成的样品具有更好的热稳定性。通过苯甲醇的选择性氧化和脱氢研究了样品的催化性能,表明BaTiO_3的高表面积可以提高总转化率和苄醛的选择性。

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