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Accelerated life time testing of fused silica upon ArF laser irradiation

机译:在ArF激光照射下加速熔融石英的使用寿命测试

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We report on two approaches to strongly shorten life time testing of fused silica's absoption degradation upon 193 nm laser irradiation. Both approaches are based on enhancing the two photon absorption (TPA) induced generation of E' and NBOH defects centers in fused silica compared to common marathon test irradiation parameters. For the first approach the irradiation fluence is increased from typical values H<1 mJ/cm~2 to H=10 mJ/cm~2, therefore increasing the peak laser power for a more efficient TPA process. To avoid microchannel formation in the samples, being a common break-down criterion in marathon tests based on transmission measurements, a small sample of 10 mm length is irradiated and the absorption is measured directly by the laser induced deflection (LID) technique. For comparing the experimental results with a real marathon test at H=1.3 mJ/cm~2, an experimental grade sample with very low hydrogen content, i.e. fast absorption changes due to reduced defect annealing, is choosen. During the fluence dependent absorption measurements after the prolonged irradiation at H=10 mJ/cm~2 it is found, that both experiments reveal very comparable absorption data for H=1.3 mJ/cm~2. For investigating standard material with high hydrogen content, i.e. slow absorption increase due to effective defect annealing, a sample is cooled down to -180 ℃ in a special designed experimental setup and irradiated at a laser fluence H=10 mJ/cm~2. To control the increase of the defect density and to determine the end of the TPA induced defect generation, the fluorescence at 650 nm of the generated NBOH centers is monitored. Before and after the low temperature experiment, the absorption coefficient is measured directly by LID technique. By applying both, elevated laser fluence and low temperature, the ArF laser induced generation of E' and NBOH centers in the investigated sample is terminated after about 1.2~*10~7 laser pulses. Therefore, a strong reduction of irradiation time is achieved in comparison to about 10~(10) pulses required in common marathon test applications.
机译:我们报告了两种方法,可大大缩短193 nm激光辐照下熔融石英吸收性能退化的寿命测试。与普通的马拉松测试辐照参数相比,这两种方法都是基于增强两个光子吸收(TPA)引起的熔融石英中E'和NBOH缺陷中心的生成。对于第一种方法,辐照通量从典型值H <1 mJ / cm〜2增加到H = 10 mJ / cm〜2,因此增加了峰值激光功率以实现更有效的TPA工艺。为了避免在样品中形成微通道(这是基于透射率测量的马拉松测试中常见的分解标准),辐照10 mm长的小样品,并通过激光诱导偏转(LID)技术直接测量吸收率。为了将实验结果与H = 1.3 mJ / cm〜2的真实马拉松试验进行比较,选择了氢含量非常低的实验级样品,即由于减少的缺陷退火而导致的快速吸收变化。在H = 10 mJ / cm〜2的长时间照射后,在依赖注量的吸收测量过程中,发现两个实验都显示出非常可比的H = 1.3 mJ / cm〜2的吸收数据。为了研究含氢量高的标准材料,即由于有效的缺陷退火而导致的缓慢吸收增加,在特殊设计的实验装置中将样品冷却至-180℃,并以激光通量H = 10 mJ / cm〜2进行辐照。为了控制缺陷密度的增加并确定TPA诱导的缺陷产生的结束,监测了所产生的NBOH中心在650 nm处的荧光。低温实验前后,吸收系数通过LID技术直接测量。通过施加提高的激光能量密度和低温,在约1.2〜* 10〜7个激光脉冲后,终止了ArF激光诱导的E'和NBOH中心的生成。因此,与普通马拉松测试应用中所需的约10〜(10)个脉冲相比,可以大大减少照射时间。

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