Identification of diazonaphthoquinone esters of polyhydroxybenzophenone compounds

机译：聚羟基二苯甲酮化合物的重氮萘醌酯的鉴定

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Abstract: The seven possible 2,1-diazonaphthoquinone-5-sulfonates of 2,3,4- trihydroxybenzophenone have been isolated and characterized by IR, chromatographic and advanced NMR techniques. HPLC procedures for their analysis are given which show counterintuitive effects in the HPLC elution sequence due to the effect of intramolecular H-bonding on the polarity of some esters. A reaction scheme is proposed which qualitatively identifies preferred pathways to the trisester. !0

机译：摘要：已分离出7种可能的2,3,4-三羟基二苯甲酮的2,1-二重氮萘醌-5-磺酸盐，并通过红外，色谱和先进的核磁共振技术对其进行了表征。给出了用于其分析的HPLC程序，由于分子内H键对某些酯的极性的影响，在HPLC洗脱序列中显示出违反直觉的效果。提出了一种反应方案，其定性地确定了通往三酯的优选途径。！0

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《Advances in Resist Technology and Processing XI》|1994年|p.696-706|共11页
会议地点 San Jose CA(US);San Jose CA(US)
作者
John DiCarlo; Hoechst Celanese Corp.; Coventry; RI; USA; O.B. Evans; Hoechst Celanese Corp.; Coventry; RI; USA; J.Fedyk; Hoechst Celanese Corp.; Somerville; NJ; USA; Stanley A. Ficner; Hoechst Celanese Corp.; Somerville; NJ; USA; Mohammad A. Khadim; Hoech;
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正文语种 eng
中图分类无线电电子学、电信技术;
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1. A simple HPLC method for determination of 2-diazonaphthoquinone-5-sulphonic acid phenyl ester used in positive photoresists [J] . Maruthi Janaki Ram Reddy, V Venkat Reddy, B Ananda Rao Indian Journal of Chemical Technology . 2006,第3期

机译：一种简单的HPLC方法测定用于正性光刻胶的2-重氮萘醌-5-磺酸苯酯
2. A simple HPLC method for determination of 2-diazonaphthoquinone-5-sulphonic acid phenyl ester used in positive photoresists [J] . Rao B Ananda, Rao V Jayathirtha, Reddy Maruthi Janaki Ram, Indian journal of chemical technology . 2006,第3期

机译：一种简单的HPLC法测定用于正性光刻胶的2-重氮萘醌-5-磺酸苯酯
3. Novel positive-working aqueous-base developable photosensitive polyimide precursors based on diazonaphthoquinone-capped polyamic esters [J] . Hsu SLC., Lee PI., King JS., Journal of Applied Polymer Science . 2003,第8期

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4. Identification of diazonaphthoquinone esters of polyhydroxybenzophenone compounds [C] . John DiCarlo, O.B. Evans, J.Fedyk Hoechst Celanese Corp. Somerville NJ USA, Conference on advances in resist technology and processing . 1994

机译：二羟基苯甲酮化合物的重氮萘醌酯的鉴定
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Identification of diazonaphthoquinone esters of polyhydroxybenzophenone compounds

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