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Analysis of Measuring Time for Au Nanoparticle Size Measurement by Photon Cross Correlation Spectroscopy

机译:光子互相关光谱法测量金纳米粒子的测量时间分析

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It introduced the basic principle of measuring the size of nanoparticles by the method of Photon crosscorrelation spectroscopy (PCCS). The measuring time for Au particle size measurement at different concentration using PCCS was studied. We measured gold particles with an average diameter of 24.5 nm at different concentration and different measuring times by PCCS. The measuring results demonstrate that for the same measuring time, the higher the concentration is, the smaller the standard deviation of repeated measurements is; for suspension of the same concentration, the longer the measuring time is, the smaller the standard deviation of repeated measurements is. It fitted the relationship between the standard deviation of measuring results and the measuring time at difference concentration. For the needed measuring accuracy, we can get the measuring time for some concentration according to the curve fitting.
机译:介绍了通过光子互相关光谱法(PCCS)测量纳米颗粒尺寸的基本原理。研究了使用PCCS在不同浓度下测量Au粒径的时间。我们通过PCCS在不同的浓度和不同的测量时间下测量了平均直径为24.5 nm的金颗粒。测量结果表明,对于相同的测量时间,浓度越高,重复测量的标准偏差越小;对于相同浓度的悬浮液,测量时间越长,重复测量的标准偏差就越小。它拟合了不同浓度下测量结果的标准偏差与测量时间之间的关系。为了获得所需的测量精度,我们可以根据曲线拟合得出某些浓度的测量时间。

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