ASTM D5453-19a Standard Test Method for Determination of Total Sulfur in Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel Engine Fuel, and Engine Oil by Ultraviolet Fluorescence

火焰点火发动机燃料柴油发动机燃料和发动机油通过紫外线荧光测定的总硫含量的标准试验方法

基本信息

标准号

ASTM D5453-19a

标准状态

现行

发布单位或类别

美国-美国材料与试验协会(US-ASTM);

发布日期

实施日期

废止日期

CCS分类

ICS分类

75.100 石油及相关技术 - 润滑剂、工业油及相关产品

研制信息

起草单位

- 展开▼

起草人

归口单位

D02.03

摘要

1.1This test method covers the determination of total sulfur in liquid hydrocarbons, boiling in the range from approximately 25 °C to 400 °C, with viscosities between approximately 0.2 cSt and 20 cSt (mm2/s) at room temperature.1.2Three separate interlaboratory studies (ILS) on precision, and three other investigations that resulted in an ASTM research report, have determined that this test method is applicable to naphthas, distillates, engine oil, ethanol, Fatty Acid Methyl Ester (FAME), and engine fuel such as gasoline, oxygen enriched gasoline (ethanol blends, E-85, M-85, RFG), diesel, biodiesel, diesel/biodiesel blends, and jet fuel. Samples containing 1.0 mg/kg to 8000 mg/kg total sulfur can be analyzed (Note 1).Note 1:Estimates of the pooled limit of quantification (PLOQ) for the precision studies were calculated. Values ranged between less than 1.0 mg/kg and less than 5.0 mg/kg (see Section9and16.1).1.3The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.For warning statements, see3.1,7.3,7.4, Section8, and9.1.1.5This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. ====== Significance And Use ======4.1Some process catalysts used in petroleum and chemical refining can be poisoned when trace amounts of sulfur bearing materials are contained in the feedstocks. This test method can be used to determine sulfur in process feeds sulfur in finished products, and can also be used for purposes of regulatory control. 1.1本试验方法包括测定液态烃中的总硫，沸腾范围约为25 °C至400 °C，粘度约为0.2 cSt和20 cSt（毫米2./s）在室温下。1.2关于精度的三项独立实验室间研究（ILS）和其他三项导致ASTM研究报告的研究已确定，本试验方法适用于石脑油、馏分油、发动机油、乙醇、脂肪酸甲酯（FAME）和发动机燃料，如汽油、富氧汽油（乙醇混合物、E-85、M-85、RFG）、柴油、生物柴油、柴油/生物柴油混合物，和喷气燃料。含有1.0的样品 mg/kg至8000 可以分析mg/kg的总硫(注1).注1:计算了精密度研究的混合定量限（PLOQ）估计值。数值范围小于1.0 mg/kg且小于5.0 毫克/千克（见第节9和16.1).1.3以国际单位制表示的数值应视为标准值。本标准不包括其他计量单位。1.4本标准并非旨在解决与其使用相关的所有安全问题（如有）。本标准的用户有责任在使用前制定适当的安全、健康和环境实践，并确定监管限制的适用性。有关警告声明，请参阅3.1,7.3,7.4部分8.和9.1.1.5本国际标准是根据世界贸易组织技术性贸易壁垒（TBT）委员会发布的《关于制定国际标准、指南和建议的原则的决定》中确立的国际公认标准化原则制定的。====意义和用途======4.1当原料中含有微量含硫材料时，用于石油和化工精炼的某些工艺催化剂可能中毒。本试验方法可用于测定过程饲料中的硫成品中的硫，也可用于监管控制。展开▼

关联标准

代替如下标准

1.ASTM D5453-19 Standard Test Method for Determination of Total Sulfur in Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel Engine Fuel, and Engine Oil by Ultraviolet Fluorescence。

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1.Standard Test Method for Determination of Total Sulfur in Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel Engine Fuel, and Engine Oil by Ultraviolet Fluorescence
机译：火焰点火发动机燃料柴油发动机燃料和发动机油通过紫外线荧光测定的总硫含量的标准试验方法
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机译：火焰点火发动机燃料柴油发动机燃料和发动机油通过紫外线荧光测定的总硫含量的标准试验方法
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