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Method for producing copper selenium nanoparticles, copper nanoparticle aggregates, copper selenium nanoparticles and film coating structure

机译:生产铜硒纳米粒子,铜纳米粒子聚集体,硒纳米粒子和薄膜涂层结构的方法

摘要

PROBLEM TO BE SOLVED: To provide a method capable of mass-producing copper selenium nanoparticles having a small half-value and half width of an absorption peak by strongly absorbing light having a wavelength in the near-infrared region. A method for producing copper selenium nanoparticles by a flow process, wherein a copper starting material and a ligand are combined to form a fluid copper precursor, and the selenium starting material is suspended in a liquid to flow. The step of forming a sex selenium precursor, the step of combining a fluid copper precursor and a fluid selenium precursor to form a fluid copper-selenium mixture, and passing the fluid copper-selenium mixture through at least one heating unit. The fluid copper-selenium mixture comprises a step of forming copper selenium nanoparticles and a step of isolating copper selenium nanoparticles in an oxygen-deficient environment, and the fluidized copper-selenium mixture contains copper selenium nanoparticles. The isolation step involves precipitating copper selenium nanoparticles by combining a solution containing copper selenium nanoparticles with a deoxidized high polar solvent, which is more polar than low polar solvents. .. [Selection diagram] Fig. 2
机译:要解决的问题:提供一种能够通过在近红外区域中具有波长的强烈吸收光而产生具有小的半值和吸收峰的半值的硒纳米粒子的方法。通过流动方法生产铜硒纳米粒子的方法,其中组合铜原料和配体以形成流体铜前体,并且硒原料悬浮在液体中以流动。形成性硒前体的步骤,将流体铜前体和流体硒前体组合形成流体铜 - 硒混合物的步骤,并通过至少一个加热单元使流体铜 - 硒混合物通过。流体铜 - 硒混合物包含形成铜硒纳米粒子的步骤,以及在缺氧环境中分离硒纳米颗粒的步骤,流化的铜 - 硒混合物含有硒纳米粒子。分离步骤涉及通过将含铜硒纳米颗粒的溶液与脱氧的高极性溶剂组合来沉淀硒纳米粒子,其比低极性溶剂更偏振。 .. [选择图]图2

著录项

  • 公开/公告号JP2021054713A

    专利类型

  • 公开/公告日2021-04-08

    原文格式PDF

  • 申请/专利权人 昭栄化学工業株式会社;

    申请/专利号JP20200165705

  • 发明设计人 ハーベン;パトリック;

    申请日2020-09-30

  • 分类号C01B19/04;B82Y30;B82Y40;

  • 国家 JP

  • 入库时间 2024-06-14 21:24:45

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