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Chromatographic device for simultaneous collection and evaporation of sequential volatile non-aqueous eluates

机译:色谱仪,用于同时收集和蒸发顺序挥发的非水洗脱液

摘要

The present disclosure relates to a chromatographic device for the simultaneous collection and evaporation of sequential volatile non- aqueous eluates. The device integrates collection and evaporation steps by continuously feeding the collected eluate directly to an evaporation vessel via a column delivery tube. As the solvent is evaporated from the evaporation vessel, eluate is continuously fed to said vessel, thereby eliminating the need for manual transfer and reducing the chances of contamination. The device increases the surface area available for evaporation, allows for the evaporation of volumes of solvent greater than the capacity of the evaporation vessel and allows for as much as a 5- fold reduction in the time necessary to carry out the chromatography and evaporation procedure.
机译:本公开涉及用于同时收集和蒸发顺序的挥发性非水洗脱液的色谱装置。该设备通过将收集的洗脱液通过色谱柱输送管连续不断地直接喂入蒸发容器中,从而整合了收集和蒸发步骤。随着溶剂从蒸发容器中蒸发,洗脱液被连续进料到所述容器中,从而消除了手动转移的需要并减少了污染的机会。该设备增加了可用于蒸​​发的表面积,允许蒸发的溶剂量大于蒸发容器的容量,并且可减少进行色谱和蒸发程序所需时间的5倍之多。

著录项

  • 公开/公告号US4228008A

    专利类型

  • 公开/公告日1980-10-14

    原文格式PDF

  • 申请/专利权人 HOFFMANN-LA ROCHE INC.;

    申请/专利号US19790027345

  • 发明设计人 ROBERT J. KAROL;RAYMOND E. GREW;

    申请日1979-04-05

  • 分类号B01D15/08;

  • 国家 US

  • 入库时间 2022-08-22 17:00:38

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