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PROCESS AND INSTALLATION FOR OBTAINING ETHANOL BY THE CONTINUOUS ACID HYDROLYSIS OF CELLULOSIC MATERIALS

机译:连续酸水解纤维素材料制取乙醇的工艺及安装

摘要

A B S T R A C TInvention Patent for a "PROCESS AND INSTALLATION FOROBTAINING ETHANOL BY THE CONTINUOUS ACID HYDROLYSISOF CELLULOSIC MATERIALS", such process comprising thestages of: providing an homogenized aqueous pulp ofcellulosic material having about 3 to 30% in weightof solids; pumping the cellulosic material pulp, ina substantially continuous way, to the interior ofthe inlet end of a tubular reactor and restrictingits outlet opposite end to maintain a given internalpressure inside the same; heating the pressurizedcellulosic material pulp up to the temperature ofabout 160 to 250°C before its introduction into thereactor; adding, in a substantially continuous way,a given dose of a concentrated acid to the pressurizedand heated cellulosic material pulp, which will becontinuously diluted in the reactor, to provide thehydrolysis reaction of said pulp, the acid additionbeing made inside the reactor at a point longitudinallyadjustable from the inlet end of the reactor; dischargingin a substantially continuous way through the outletend of the reactor a given load of hydrolyzed cellulosicmaterial, said discharge being regulated in conjunctionwith the longitudinal positioning of the point ofaddition of the acid, thus fixing the reaction timeadequate for the cellulosic material pulp; subjectingthe hydrolyzed cellulosic material pulp to an abruptpressure drop and cooling immediately after it leavesthe reactor; neutralizing and fermenting the resultingaqueous solution to obtain ethanol; and recovering theresulting byproducts which are methanol, furfural, aceticacid and lignin.
机译:A B S T R A C T“针对以下产品的过程和安装”的发明专利通过连续酸水解获得乙醇纤维素材料”,这种方法包括阶段:提供均质的纸浆重量约为3%至30%的纤维素材料固体泵入纤维素材料浆基本上连续的方式管式反应器的进口端它的出口相对端保持给定的内部内部压力相同;加热加压纤维素材料浆温度大约160至250°C的温度,然后再引入反应堆;以基本上连续的方式添加给定剂量的浓酸和加热的纤维素材料纸浆,这将是在反应器中连续稀释,以提供所述纸浆的水解反应,酸加成在反应堆内部纵向放置从反应器的进口端可调节;放电以基本连续的方式通过出口给定负载量的水解纤维素物料,所述排放量要同时进行调节与点的纵向定位添加酸,从而固定反应时间足够用于纤维素材料纸浆;服从水解的纤维素原料浆突然变硬离开后立即降压并冷却反应堆;中和发酵产物水溶液获得乙醇;并恢复产生的副产物为甲醇,糠醛,乙酸酸和木质素。

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