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Sensor for hand held gas chromatograph

机译:手持式气相色谱仪传感器

摘要

A portable gas chromatographic detector includes two identical platinum coils mounted on identically aligned conducting posts. One coil is placed in an occluded chamber; the other coil is placed in an identical isolated chamber. Both coils have connection to legs of a bridge circuit and have substantially identical current flow passed along their length. Both chambers are preferably identically dimensioned and are large enough not to interfere with the field of the coils. The occluded chamber communicates through a short passageway with a passing classified gas stream from a chromatographic column. It has been found that the motion with respect to one coil is compensated with respect to the motion with the remaining coil so that the only differential in electrical resistance measured across the bridge circuit is that induced by the cooling property of helium on the heated coil in the occluded chamber. Cycling of the portable chromatograph includes a first short cycle. In the absence of detected helium, the instrument immediately returns to a standby state in readiness for a closely repeated cycle. Upon the detection of helium, a second and longer cycle results prolonged only by that time interval necessary for measurement of the helium and purging helium residual from the instrument collection conduits. For rich helium measurement resulting in super cooling of the occluded coil, a reverse bias is applied to the isolated coil through the bridge circuit to induce a warming current charge to the supercooled occluded coil. This enables rapid repeated measurement without prolonged warm-up intervals which would be otherwise required.
机译:便携式气相色谱检测器包括两个相同的铂线圈,安装在相同对齐的导电柱上。一个线圈放置在一个封闭的腔室中。另一个线圈放置在相同的隔离室中。两个线圈均连接至桥式电路的分支,并且沿其长度流经的电流基本相同。两个腔室优选地具有相同的尺寸,并且其大小足够大以不会干扰线圈的磁场。闭塞腔室通过短通道与来自色谱柱的经过分级的气流连通。已经发现,相对于一个线圈的运动相对于其余线圈的运动得到补偿,从而跨桥电路测得的唯一电阻差是由氦在加热线圈上的冷却特性引起的。封闭的房间。便携式色谱仪的循环包括第一个短循环。在没有检测到氦气的情况下,仪器立即返回待机状态,准备好进行紧密重复的循环。一旦检测到氦气,第二个周期和更长的周期结果只会延长测量氦气和清除仪器收集导管中残留的氦气所需的时间间隔。对于富氦测量导致闭塞线圈过冷,将反向偏压通过电桥电路施加到隔离线圈上,以向过冷闭塞线圈感应出暖流电荷。这样可以快速重复进行测量,而无需延长预热间隔。

著录项

  • 公开/公告号US4787239A

    专利类型

  • 公开/公告日1988-11-29

    原文格式PDF

  • 申请/专利权人 MARK PRODUCTS INC.;

    申请/专利号US19880142120

  • 发明设计人 RICHARD DIMATTEO;

    申请日1988-01-11

  • 分类号G01N30/66;

  • 国家 US

  • 入库时间 2022-08-22 06:28:51

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