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Process for working up the filtration residue of crude sodium prepared by fusion electrolysis into a high-purity sodium alcholate

机译:处理通过熔融电解制得的高纯度胆酸钠的粗钠滤渣的方法

摘要

A process for converting the filtration residue of crude sodium produced by fusion electrolysis into a sodium alcoholate with a low NaOH content. The residue first is intensively and continuously mixed for 2-5 hours at 300°-600° C. and then is added with stirring to the particular alcohol, possibly with heat added. The alcoholate solution so formed is filtered and the alcoholate may be obtained from the filtrate by distilling off the solvent.
机译:一种将通过熔融电解产生的粗制钠的过滤残余物转化为具有低NaOH含量的醇钠的方法。首先将残余物在300°-600°C下剧烈连续混合2-5小时,然后在搅拌下将其加入到特定的醇中,可能需要加热。过滤如此形成的醇化物溶液,并可以通过蒸馏除去溶剂而从滤液中获得醇化物。

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