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PRODUCTION OF SINGLE CRYSTAL

机译:单晶生产

摘要

PURPOSE:To easily and stably obtain single crystal by passing the sintered rod for a raw material through the inside of an infrared convergent band melting furnace at high speed and making the sintered rod uniform and dense and thereafter passing the same through the inside of the furnace at low speed and crystallizing it in the case of using the melting furnace and growing single crystal in a band melting method. CONSTITUTION:MgO and Al2O3 are mixed with oxides of lanthanoid elements at such a ratio that single crystal having composition of LnMgAl11O19 (Ln shows lanthanoid elements of La, Ce, Pr, Nd, Sm, Eu, Gd and solid solution thereof) is obtained. The sintered rod for a raw material is produced by forming this mixture and heat-treating the formed body. Then this sintered rod is melted in an infrared convergent band melting furnace equipped with the halogen lamps 4, a quartz pipe 3 and a rotary ellipsoidal mirror 5 or the like. This melt is once passed through a zone at 30-70mm/h speed and the uniform and dense raw material rod M is produced. Then the obtained raw material rod M is again melted in the furnace. While this melt is brought into contact with a seed crystal S, it is passed through the zone at 1-4mm/h. Single crystal of LnMgAl11O19 is grown by a band melting method.
机译:目的:通过使原料烧结棒高速通过红外会聚熔化炉内部并使烧结棒均匀致密,然后使其通过炉子内部,从而轻松,稳定地获得单晶在使用熔化炉并以能带熔化法生长单晶的情况下,以低速结晶。组成:MgO和Al2O3与镧系元素的氧化物以一定比例混合,从而获得具有LnMgAl11O19组成的单晶(Ln显示镧系元素La,Ce,Pr,Nd,Sm,Eu,Gd及其固溶体)。通过形成该混合物并热处理成型体来制造用于原料的烧结棒。然后,该烧结棒在配备有卤素灯4,石英管3和旋转椭球镜5等的红外会聚带熔化炉中熔化。该熔体一次以30-70mm / h的速度通过一个区域,从而产生均匀且致密的原料棒M。然后,将获得的原料棒M再次在炉中熔化。当该熔体与籽晶S接触时,它以1-4mm / h的速度通过该区域。 LnMgAl11O19的单晶通过能带熔化法生长。

著录项

  • 公开/公告号JPH04338191A

    专利类型

  • 公开/公告日1992-11-25

    原文格式PDF

  • 申请/专利权人 NEC CORP;

    申请/专利号JP19910138440

  • 发明设计人 NAKABAYASHI YUKINOBU;

    申请日1991-05-14

  • 分类号C30B13/32;C30B29/22;H01L21/208;

  • 国家 JP

  • 入库时间 2022-08-22 05:17:47

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