首页> 外国专利> PROCESS FOR PREPARING BIOMEDICAL GRADE CHITIN AND CHITOSAN

PROCESS FOR PREPARING BIOMEDICAL GRADE CHITIN AND CHITOSAN

机译:生物医药级甲壳素和壳聚糖的制备方法

摘要

The present invention provides a process for preparing a biomedical grade chitin of a high purity and whiteness with a high molecular weight and a biomedical grade chitosan of a high degree of deacetylation and high molecular weight from the chitin produced in accordance with the present invention. Specifically, the process for preparation of the chitin in accordance with the present invention comprises the steps of: (A) drying crustaceous shells and crushing the dried shells to provide a finely crushed powder; (B) digesting initially the powder in a HCl solution at a temperature ranging from -10 to 10.degree.C for a period ranging from 10 to 25 hours and, thereafter, further digesting the powder in the HCl solution at a temperature ranging from 10 to 20.degree.C for a period ranging from 2 to 8 hours; (C) washing with water, filtering, rinsing with a an organic solvent and drying the HCl-treated material to provide a crude chitin; (D) soaking and heating the crude chitin in a NaOH solution; and (E) washing with water, filtering, rinsing with the organic solvent and drying the NaOH-treated chitin to obtain the high purity chitin.
机译:本发明提供了由根据本发明生产的甲壳质制备具有高分子量的高纯度和白度的生物医学级甲壳质以及具有高度脱乙酰度和高分子量的生物医学级甲壳质的方法。具体地,根据本发明的几丁质的制备方法包括以下步骤:(A)干燥甲壳并粉碎干燥的壳以提供细碎的粉末; (B)首先在-10℃至10℃的温度范围内的HCl溶液中消化粉末,持续10至25小时,此后,在80℃至70℃的温度范围内进一步消化粉末。 10至20摄氏度,持续2至8个小时; (C)用水洗涤,过滤,用有机溶剂冲洗并干燥用HCl处理过的物质,得到粗壳多糖。 (D)将粗几丁质在NaOH溶液中浸泡并加热; (E)用水洗涤,过滤,用有机溶剂冲洗并干燥经NaOH处理的甲壳质以获得高纯度甲壳质。

著录项

  • 公开/公告号CA2101079A1

    专利类型

  • 公开/公告日1994-08-09

    原文格式PDF

  • 申请/专利权人 JEON DONG-WON;

    申请/专利号CA19932101079

  • 发明设计人 JEON DONG-WON;

    申请日1993-07-21

  • 分类号C08B37/08;

  • 国家 CA

  • 入库时间 2022-08-22 04:42:26

相似文献

  • 专利
  • 外文文献
  • 中文文献
获取专利

客服邮箱:kefu@zhangqiaokeyan.com

京公网安备:11010802029741号 ICP备案号:京ICP备15016152号-6 六维联合信息科技 (北京) 有限公司©版权所有
  • 客服微信

  • 服务号