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Secondary ion mass spectrometry and preparation manner null of the standard reference material which is used for
Secondary ion mass spectrometry and preparation manner null of the standard reference material which is used for
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机译:二次离子质谱法及其制备方法无用于本标准的标准参考物质
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摘要
A method of analyzing a solid, metal-containing sample by secondary ion mass spectrometry for the determination of the concentration of the metal, wherein the sample is shaped into a disc and measured for the metal ion intensity of secondary ion mass spectrometry. The disc is prepared by a process including the steps of: (a) mixing the sample with a liquid to dissolve the metal; (b) separating the metal from the solution as solids to form a first solid mass containing the metal; (c) calcining the solid mass to convert the metal into an oxide and to obtain a second solid mass; (d) mixing the second solid mass with silver powder in an amount of 0.15-5 parts by weight per part by weight of the metal oxide to obtain a mixture having a particle size of not greater than 100 mu m; and (e) shaping the mixture into the disc. When the sample is a liquid, the steps (a) and (b) are omitted. This technique is applicable for the preparation of a standard sample having a known composition of metals used for constructing a calibration curve.
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