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Process for chromatographic analysis of aliphatic olefinic alcohol, acetates and ketones

机译:脂族烯烃醇,乙酸酯和酮的色谱分析方法

摘要

The invention can be utilized in the agriculture. The analysis is made to a chromatograph with a flame ionozation detector and a capilary glass column of 51 m 0,25 mm with an efficiency of 93264 of theoretical plates according to the dodecan. On the inner surface of the column pretreated with hydrofluoric acid and methanol potassium hydroxide solution by means of the statical method under high pressure is being applied the stationary phase of liquid crystal cholesteryl-n-met-hoxyben-zoate. The isomers are separated at the mesophase existance temperature of 170...190 C, at the evaporator temperature of 200 C into the nitrogen carrier gas flow at the flow separation of 1:50. Claims: 1
机译:本发明可用于农业。使用带有火焰离子化检测器和51 m 0,25 mm毛细管玻璃柱的色谱仪进行分析,根据dodecan,理论塔板的效率为93264。在高压下通过静态方法在用氢氟酸和甲醇氢氧化钾溶液预处理的柱的内表面上施加液晶胆固醇-正-间-羟基苯甲酸酯-液晶的固定相。在170 ... 190 C的中间相存在温度下,在200 C的蒸发器温度下,异构体被分离为氮气载气流,流动分离率为1:50。索赔:1

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