METODE MODERNISASI IN-SITU PADA REAKTOR SINTESIS EKSOTERMIS HETEROGEN

摘要

A method for in-situ modernization of a heterogeneous exothermic synthesis reactor, comprising the steps of providing at least a first and at least a second catalytic bed (12,13) in an upper (2a) respectively lower (2b) portion of the reactor, providing additionally a lowermost catalytic bed (14) in the lower portion (2b) of the reactor having a reaction volume smaller than the reaction volume of the second catalytic bed (13), and loading the lowermost catalytic bed (14) with a catalyst having an activity higher than the activity of the catalyst loaded in the other beds (12,13), this catalyst preferably based on graphite-supported ruthenium. Thanks to the above steps, the present method allows to obtain a reactor with high conversion yield.