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Process for preparing sodium formaldehyde sulfoxylate

机译:甲醛次硫酸氢钠的制备方法

摘要

Zinc dust is mixed with water and added with soluble cadmium salt, whereupon at room temperature to 45.degree. C adds SOi2 and removed after the reduction is treated with formaldehyde, whereupon, after the disproportionation, the second time with added zinc dust and a second reduction, added with sodium hydroxide and finally the usual finishing of the product. Sul dvojmocnéhokadmia was added in an amount of 0.03 to 0.08, optimally from 0.035 to 0.045 g of cadmium per 100 g of zinc dust, based on the weight of zinc powder in the starting aqueous slurry, and it is preferably a sulphate, chloride, acetate or cadmium. Preferably a zinc powder containing less than 96 wt%. kovovéhozinku, of dp 9-20 .mi.ma retained on a 0.06 mm at most 0.5 wt%.
机译:锌粉与水混合,并加入可溶性镉盐,然后在室温至45.degree。 C添加SO 2并在还原后用甲醛处理,然后歧化后,第二次添加锌粉,第二次还原,添加氢氧化钠,最后按常规方法精制,除去C。 dvojmocnéhokadmia的添加量为每100克锌粉中的0.03至0.08镉,最理想的是从0.035至0.045 g镉,基于起始水性浆料中锌粉的重量,优选为硫酸盐,氯化物,乙酸盐或镉。优选地,锌粉的含量小于96重量%。 dp 9-20 .ma.ma的kovovéhozinku保留在0.06 mm处,最多0.5 wt%。

著录项

  • 公开/公告号CZ2006495A3

    专利类型

  • 公开/公告日2008-02-20

    原文格式PDF

  • 申请/专利权人 HCHZ-CHEMIE HRUUEOV A. S.;

    申请/专利号CZ19950020064

  • 发明设计人 STABRYN JAROSLAV;DINKOV TOMAUE;

    申请日2006-08-07

  • 分类号C07C313/02;

  • 国家 CZ

  • 入库时间 2022-08-21 20:08:28

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