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METHOD OF PRODUCING RARE EARTH-TRANSITION METAL-NITROGEN-BASED MAGNET POWDER, RESULTANT RARE EARTH-TRANSITION METAL-NITROGEN-BASED MAGNET POWDER, AND COMPOSITION FOR BOND MAGNET USING THE SAME, AND BOND MAGNET USING THE SAME
METHOD OF PRODUCING RARE EARTH-TRANSITION METAL-NITROGEN-BASED MAGNET POWDER, RESULTANT RARE EARTH-TRANSITION METAL-NITROGEN-BASED MAGNET POWDER, AND COMPOSITION FOR BOND MAGNET USING THE SAME, AND BOND MAGNET USING THE SAME
PROBLEM TO BE SOLVED: To provide production capable of safely, inexpensively and safely producing rare-earth transition metal-nitrogen-based magnet powders by a reduction diffusion method without reducing magnetic characteristics, and without using gaseous hydrogen or causing a reduced product to disintegrate by reducing an amount of use, a composition for a bond magnet using the same, and a bond magnet capable of making various apparatuses smaller in sizes and higher in characteristics.;SOLUTION: The production method of the rare-earth transition metal-nitrogen-based magnet powder comprising using water or water and gaseous hydrogen in the disintegration in a step of mixing transition metal alloy powder, rare earth oxide powder, and a reducing agent for reducing the rare earth oxide powder, and subjecting the mixture to heating calcination in a non-oxidizing atmosphere to form a reduction diffusion reaction product, then causing the resultant reduced product to disintegrate and expressed by the following formula (1) is provided. RxFe(100-x-y-z)MyNz(1) (In the formula, R denotes rare earth element, M denotes a rare-earth transition metal selected from the group consisting of Cu, Mn, Cr, Ti, Ni and Zr; x. y, z satisfy, by atomic %, 4≤x≤18%, 0.3≤y≤23%, and 15≤z≤25%).;COPYRIGHT: (C)2009,JPO&INPIT
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机译:要解决的问题:提供一种能够通过还原扩散方法安全,廉价且安全地生产稀土过渡金属-氮基磁铁粉末的生产方法,而不会降低磁特性,并且无需使用气态氢或导致还原产物崩解。减少使用量,用于粘结磁铁的组合物以及能够使各种装置小型化,高特性化的粘结磁铁。解决方案:稀土过渡金属-氮系的制造方法磁铁粉末,其包括在将过渡金属合金粉末,稀土氧化物粉末和用于还原稀土氧化物粉末的还原剂混合并在非加热条件下进行加热煅烧的步骤中分解使用水或水和气态氢。 -氧化气氛形成还原扩散反应产物,然后使所得的还原产物分解并表达提供以下公式(1)。 R x Sub> Fe (100-xyz) Sub> M y Sub> N z Sub>(1)(在公式中,R表示稀土元素,M表示选自Cu,Mn,Cr,Ti,Ni和Zr的稀土过渡金属; x.y,z原子百分比满足4%x 18%,0.3%le ; y≤ 23%和15≤ z≤ 25%)。;版权所有:(C)2009,JPO&INPIT
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