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PROCESS FOR MAKING ANATASE TITANIUM (IV) OXIDE

机译:制备锐钛型二氧化钛的工艺

摘要

The disclosure pertains to a process for making anatase titanium dioxide particles, comprising: vigorously mixing (a) a volume of a first component comprising a major proportion of an alcohol, a minor proportion of a titanium alkoxide and a minor proportion of a titanium alkoxide activator selected from the group consisting of water and a first aqueous base, and (b) a second component selected from the group consisting of water and a second aqueous base, at least one of the first component or the second component having a base therein, the second component being substantially free of alcohol, to form a mixture comprising a suspension of finely divided titanium (IV) oxide particles, the mixture having a water to titanium molar ratio ranging from about 40 to about 1 to about 5000 to about 1, wherein the proportion of the titanium alkoxide, the proportion of the activator, the mixing vigor, and a ratio of the volume of the first component to the second component are effective for the suspension of the finely divided titanium (IV) oxide particles to form in the mixture; and heating the suspension to convert the titanium (IV) oxide particles of the suspension to anatase titanium dioxide.
机译:本公开内容涉及一种制备锐钛矿型二氧化钛颗粒的方法,该方法包括:剧烈混合(a)一定体积的第一组分,该第一组分包含大部分的醇,少量的钛醇盐和少量的钛醇盐活化剂。 (b)选自水和第二水性碱的第二组分,其中第一组分或第二组分中的至少一个在其中具有碱,第二组分基本上不含醇,以形成包含细分的氧化钛(IV)颗粒悬浮液的混合物,该混合物的水钛摩尔比为约40至约1至约5000至约1,其中烷氧基钛的比例,活化剂的比例,混合力以及第一组分与第二组分的体积比对悬浮液有效。细碎的氧化钛(IV)颗粒形成混合物。加热悬浮液以将悬浮液的氧化钛(IV)颗粒转化为锐钛矿型二氧化钛。

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