首页> 外国专利> THERMAL DISSOLUTION CATALYSIS METHOD FOR PREPARING LIQUID FUEL FROM LIGNITE AND THE CATALYST AND THE SOLVENT SUITABLE FOR THE METHOD

THERMAL DISSOLUTION CATALYSIS METHOD FOR PREPARING LIQUID FUEL FROM LIGNITE AND THE CATALYST AND THE SOLVENT SUITABLE FOR THE METHOD

机译:由褐铁矿和催化剂制备液体燃料的热溶解催化方法及适用的溶剂

摘要

The present invention relates to coal chemical processing, and particularly to a thermal dissolution catalysis method for preparing liquid fuel from lignite. The method comprises steps of: 1) crushing and drying lignite into coal powder; 2) stirring and mixing coal powder, a solvent and a catalyst sufficiently to form coal slurry, wherein there are 30-40% mass of coal powder, 60-70% mass of solvent, and 0.5-1% mass of catalyst relative to coal powder mass; 3) subjecting the coal slurry to thermal dissolution catalysis reaction to obtain thermal dissolution liquefied product, wherein the reaction is carried out for 30-60 minutes at a temperature 390-450° C. under a pressure 5.0-9.0 MPa; 4) separating the thermal dissolution liquefied product into gas, liquid and solid phases; and 5) upgrading the liquid product into liquid fuel. The present invention further discloses a catalyst and a solvent for use in the above method. The method according to the present invention requires moderate operation conditions and can enable organic matter in the lignite to convert at a relatively high level, the liquid fuel product, after being processed, can be used to prepare engine fuel meeting a national standard; the method requires a simple preparation apparatus, a small investment and a low cost and is a coal liquefying method meeting China's status quo.
机译:用褐煤制备液体燃料的热溶解催化方法技术领域本发明涉及煤化学加工,尤其涉及一种用褐煤制备液体燃料的热溶解催化方法。该方法包括以下步骤:1)将褐煤粉碎并干燥成煤粉; 2)充分搅拌并混合煤粉,溶剂和催化剂以形成煤浆,其中煤粉的质量为煤的30-40%,溶剂的质量为60-70%,催化剂的质量为煤的0.5-1%。粉末质量3)使煤浆进行热溶解催化反应,得到热溶解液化产物,其中,反应在390-450℃,5.0-9.0MPa的压力下进行30-60分钟。 4)将热溶解液化产物分离成气相,液相和固相; 5)将液体产品升级为液体燃料。本发明还公开了用于上述方法的催化剂和溶剂。根据本发明的方法需要适度的操作条件,并且能够使褐煤中的有机物以相对较高的水平转化,该液体燃料产品经过处理后,可以用于制备符合国家标准的发动机燃料。该方法要求制备设备简单,投资少,成本低,是一种符合中国现状的煤液化方法。

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