首页> 外国专利> Process for analyzing low molecular weight organic compound having at most 20 carbon atoms in a water/oil repellent compositon

Process for analyzing low molecular weight organic compound having at most 20 carbon atoms in a water/oil repellent compositon

机译:拒水拒油复合材料中具有最多20个碳原子的低分子量有机化合物的分析方法

摘要

Provided is a process whereby a low molecular weight organic compound having at most 20 carbon atoms present in a trace amount in a water/oil repellent composition can be analyzed accurately.;A process for analysis which comprises (a) a step of mixing a water/oil repellent composition in which a fluorinated polymer having repeating units based on a compound having a perfluoroalkyl group is dispersed or dissolved in a medium, and a C1-5 alcohol, and agglomerating the fluorinated polymer to obtain a liquid containing agglomerates of the fluorinated polymer, (b) a step of subjecting the liquid containing the agglomerates of the fluorinated polymer to solid-liquid separation to obtain a liquid phase, and (c) a step of measuring the concentration of a low molecular weight organic compound having at most 20 carbon atoms in the liquid phase by means of LC-MS, LC-MS/MS or GC-MS.
机译:提供了一种方法,通过该方法可以准确地分析在拒水拒油组合物中存在的痕量的碳原子数至多为20的低分子量有机化合物。分析方法包括(a)混合水的步骤剂/拒油组合物,其中具有基于具有全氟烷基的化合物的重复单元的氟化聚合物分散或溶解在介质中和C 1-5 醇中,并使该氟化聚合物凝聚而获得含有氟化聚合物的附聚物的液体,(b)使含有氟化聚合物的附聚物的液体进行固液分离而得到液相的步骤,以及(c)测定低分子浓度的步骤。通过LC-MS,LC-MS / MS或GC-MS在液相中具有最多20个碳原子的有机化合物。

著录项

  • 公开/公告号US2010270466A1

    专利类型

  • 公开/公告日2010-10-28

    原文格式PDF

  • 申请/专利权人 SATOSHI HIKIMA;

    申请/专利号US20100801802

  • 发明设计人 SATOSHI HIKIMA;

    申请日2010-06-25

  • 分类号B01D59/44;

  • 国家 US

  • 入库时间 2022-08-21 18:55:51

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