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SILICON DIOXIDE SYNTHESIS REACTOR AND METHOD OF PRODUCING SILICON DIOXIDE THROUGH FLAME HYDROLYSIS

机译:二氧化硅合成反应器及通过火焰水解制备二氧化硅的方法

摘要

FIELD: chemistry.;SUBSTANCE: invention can be used in synthesis of finely dispersed powder of silicon dioxide by burning liquid silicon-containing compounds in a flame of combustion gases. The method of producing silicon dioxide involves hydrolysis of silicon-containing liquids in a hydrogen medium in the presence of heated air, which is fed into the combustion zone through the centre channel of a burner at the speed of sound. The reactor consists of a horizontal cylindrical housing 1, a burner 2, which includes a channel 14 and an annular channel 15, a unit for controlling and letting in reacting flows, a flame stabiliser, an inlet pipe for mixture of exhaust gases and silicon dioxide 16. The unit for controlling and letting in reacting flows has a channel 3 which carries liquid silicon-containing compounds, a centre channel 4 which carries air, a channel 5 which carries hydrogen and a channel 6 which carries nitrogen. The flame stabiliser is placed coaxially with the burner and is made from two pipes: an outer pipe 7, which is made in form of a de Laval nozzle and consists of a confuser 9 and a diffuser 10 with perforations 13, and an inner pipe 8. The diffuser 10 has a jacket which is divided into two sections 11 and 12. The stabiliser in the assembly and its inner pipe 8 are made with possibility of displacement on a common axis.;EFFECT: invention increases efficiency of the synthesis process and quality of silicon dioxide.;6 cl, 1 dwg, 4 ex
机译:发明领域:本发明可以通过在燃烧气体的火焰中燃烧液态含硅化合物来用于合成二氧化硅的细分散粉末。生产二氧化硅的方法包括在加热的空气存在下在氢介质中水解含硅液体,该空气以声速通过燃烧器的中心通道送入燃烧区。该反应器由水平的圆柱形壳体1,燃烧器2组成,燃烧器2包括通道14和环形通道15,用于控制和允许反应流的单元,火焰稳定器,用于废气和二氧化硅的混合物的入口管。 16.用于控制和允许反应流的单元具有:通道3,其承载液态含硅化合物;中心通道4,其承载空气;通道5,其承载氢;以及通道6,其承载氮。火焰稳定器与燃烧器同轴放置,并由两根管子制成:外管7(由德拉瓦勒喷嘴形式制成,由保险管9和带有穿孔13的扩散器10组成)和内管8扩散器10具有被分成两个部分11和12的夹套。组件中的稳定器及其内管8可以在同一轴线上位移;效果:本发明提高了合成过程的效率和质量二氧化硅; 6厘升,1载重吨,4防爆

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