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METHOD AND DEVICE FOR REMOVING PHOSPHORUS IMPURITY OR BORON IMPURITY FROM LIQUID POLYCHLOROSILANE AND AGENT FOR REMOVING PHOSPHORUS IMPURITY OR BORON IMPURITY FROM LIQUID POLYCHLOROSILANE
METHOD AND DEVICE FOR REMOVING PHOSPHORUS IMPURITY OR BORON IMPURITY FROM LIQUID POLYCHLOROSILANE AND AGENT FOR REMOVING PHOSPHORUS IMPURITY OR BORON IMPURITY FROM LIQUID POLYCHLOROSILANE
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机译:从液态多氯硅烷除去磷杂质或硼杂质的方法和装置以及从液态多氯硅烷除去磷杂质或硼杂质的试剂
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摘要
PROBLEM TO BE SOLVED: To provide a method and device for removing phosphorus impurities or boron impurities from crude liquid polychlorosilanes in a manufacturing process for obtaining a high-purity silicon crystal from metal class silicon, and to provide a removing agent.;SOLUTION: The removing method comprises contacting an activated carbon having an average grain size of 0.3-1.00 mm, having a volume of fine pores of ≤0.10 mL/g of a diameter of fine pores of 50-22,500 nm according to the method of mercury intrusion method, having a diameter of fine pores of 100-400 nm at the peak of the volume of fine pores in the diameter of fine pores of ≥50 nm, having a specific surface area measured by the BET method of ≥1,300 m2/g, having a filling density of ≥0.55 g/mL, having strongly heated residues of ≤0.5 mass%, having a dust incidence by water shake tests of ≤600 ppm (mass/mass), and a hardness of ≥99.5%, with the liquid polychlorosilanes.;COPYRIGHT: (C)2011,JPO&INPIT
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