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Equipment and method for measuring sorption isotherms of gases at high pressures and supercritical fluids.

机译:用于测量高压气体和超临界流体的吸附等温线的设备和方法。

摘要

Equipment and method for measuring sorption isotherms of gases at high pressures and supercritical fluids. The equipment comprises: a distributor, at least one sample cell, a gas source, a vacuum source, a pressure sensor to measure manifold pressure and the sample cell, a set of conduits and shutoff valves which connect parts of the equipment mentioned.; The method described allows obtaining accurately the amount of gas sorbed by a sample to pressures of several thousand atmospheres over a wide temperature range considering the state of the gas can not be well described by the law of ideal gas, which may have gas sorption calibration in determining the volume of the sample cell and / or that it can not be entirely temperature analysis.
机译:用于测量高压气体和超临界流体的吸附等温线的设备和方法。该设备包括:分配器,至少一个样品池,气体源,真空源,测量歧管压力的压力传感器和样品池,连接上述设备的一部分的一组导管和截止阀。考虑到无法通过理想气体定律很好地描述气体的状态,所描述的方法可以在宽温度范围内准确获得样品在几千个大气压下吸附的气体的量,而理想的气体定律可以对气体进行校准确定样品池的体积和/或不能完全进行温度分析。

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