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METHOD FOR PROCESSING SUN FLOWER INTO PECTIN

机译:将太阳花加工成果胶的方法

摘要

The invention relates to technology of pectin production from vegetable materials, in particular to an effective method of isolating sun flower pectin and can be used in producing products of prophylactic and medical purpose and also in food and pharmaceutical industries. The invention is aimed at reducing contact time of vegetable material with acidic solutions in the process of pretreatment thereof and hydrolysis thereof in producing pectin from sun flower, reducing medium acidity, increasing production yield and improving the quality of the final product. A method of processing sun flower into pectin comprises grinding thereof, pretreatment by sodium salt solution, hydrolysis-extraction of a solid phase in a dynamic regime of hydrochloric acid (pH 1.6±5.5) with hydromodulus 1:20 and short-time contact of a pectin solution (5-10 min.) with heating to 85-120°C, gravity separation of a liquid phase, centrifugation, ultrafiltration concentration and deposition by ethanol. There provided a process scheme of continuous extractors for pretreatment of raw material and its hydrolysis by a dynamic method: salt (1) or acid (2) solution is pumped into extraction columns (4, 5, 6) where pectin substances (7) are released and the extract proceeds to further treatment (8). The solution flow rate is regulated according to column's parameters that is depending on their length and diameter so that the contact time of the isolated product not exceeding 10-30 minutes in case of using common columns. It is more preferable to use streamline extractors in a commercial process since they provide to easily extract pectins by fractions. The invention permits to increase production yield and improve the quality of final product (molecular mass, amount of galacturonic acid and rate of etherification) and also safe economic costs in pectin production due to low reagent's cost used in pretreatment of raw materials.
机译:本发明涉及从植物原料中生产果胶的技术,特别是一种分离太阳花果胶的有效方法,可用于生产预防和医疗用途的产品,也可用于食品和制药工业。本发明旨在减少植物材料在其预处理过程中与酸性溶液的接触时间,并减少其在从向日葵花中生产果胶的过程中的水解,降低中等酸度,提高产量并改善最终产品的质量。一种将向日葵花加工成果胶的方法,包括对其进行研磨,通过钠盐溶液进行预处理,在动态模数为1的盐酸(pH 1.6±5.5)的动态条件下水解萃取固相以及短时间地与果胶接触。果胶溶液(5-10分钟),加热到85-120°C,液相重力分离,离心,超滤浓缩并用乙醇沉淀。提供了一种用于动态预处理原料及其水解的连续萃取器的工艺方案:将盐(1)或酸(2)溶液泵入萃取塔(4、5、6),其中果胶物质(7)释放,提取物进行进一步处理(8)。溶液流速根据色谱柱的参数进行调节,该参数取决于色谱柱的长度和直径,因此在使用普通色谱柱的情况下,分离出的产物的接触时间不会超过10-30分钟。更优选在工业过程中使用流线型提取器,因为它们提供了容易地将果胶分馏的方式。由于用于原料预处理的试剂成本低,本发明可以提高产量并改善最终产品的质量(分子量,半乳糖醛酸的量和醚化速率),并且还可以安全地经济生产果胶。

著录项

  • 公开/公告号EA016871B1

    专利类型

  • 公开/公告日2012-08-30

    原文格式PDF

  • 申请/专利权人 ZAJNIDDIN KAMAROVICH;

    申请/专利号EA20090000674

  • 发明设计人 ZAJNIDDIN KAMAROVICH;L. FISHMAN;SHU LYU;

    申请日2009-05-05

  • 分类号C08B37/06;A23L1/0524;

  • 国家 EA

  • 入库时间 2022-08-21 17:24:58

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