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Manufacturing method of nano zinc oxide powders by hydrothermal method

机译:水热法制备纳米氧化锌粉的方法

摘要

PURPOSE: A method for manufacturing nano zinc oxide powder is provided to synthesize various types of nano-size zinc oxide powder by varying a starting material and precipitant. CONSTITUTION: A method for manufacturing 100-200nm nano zinc oxide powder of a plate and needle shape comprises a step of performing hydrothermal treatment of Zn(NO3)26H2O as a starting material and NaOH as a precipitant using cyclohexylamine as a reaction controller at 200-250C for 2-10 hours. A method for manufacturing spherical nano zinc oxide powder of 50 nm or less comprises the steps of: performing hydrothermal treatment of Zn(CH3COO)22H2O as a starting material and urea as a precipitant at 120-220C for 5-12 hours; and heat treating them at 250-300C for 12 hours.
机译:目的:提供一种用于制造纳米氧化锌粉末的方法,以通过改变起始材料和沉淀剂来合成各种类型的纳米尺寸的氧化锌粉末。组成:一种制造100-200nm板状和针状纳米氧化锌粉末的方法,包括以下步骤:在200-200℃下,以环己胺为反应控制器,对Zn(NO3)26H2O作为起始原料和NaOH作为沉淀剂进行水热处理。 250°C 2-10小时。 50nm以下的球形纳米氧化锌粉末的制造方法包括以下步骤:在120-220℃下对作为原料的Zn(CH3COO)22H2O和作为沉淀剂的尿素进行5-12小时的水热处理;并在250-300°C下热处理12小时。

著录项

  • 公开/公告号KR101108691B1

    专利类型

  • 公开/公告日2012-01-25

    原文格式PDF

  • 申请/专利权人

    申请/专利号KR20080076534

  • 申请日2008-08-05

  • 分类号B82B3;B82Y40;

  • 国家 KR

  • 入库时间 2022-08-21 17:08:40

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