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首页> 外文期刊>Journal of nanomaterials >Rapid Hydrothermal Synthesis of Zinc Oxide Nanowires by Annealing Methods on Seed Layers
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Rapid Hydrothermal Synthesis of Zinc Oxide Nanowires by Annealing Methods on Seed Layers

机译:种子层退火法快速水热合成氧化锌纳米线

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Well-aligned zinc oxide (ZnO) nanowire arrays were successfully synthesized on a glass substrate using the rapid microwave heating process. The ZnO seed layers were produced by spinning the precursor solutions onto the substrate. Among coatings, the ZnO seed layers were annealed at 100℃ for 5 minutes to ensure particle adhesion to the glass surface in air, nitrogen, and vacuum atmospheres. The annealing treatment of the ZnO seed layer was most important for achieving the high quality of ZnO nanowire arrays as ZnO seed nanoparticles of larger than 30 nm in diameter evolve into ZnO nanowire arrays. Transmission electron microscopy analysis revealed a single-crystalline lattice of the ZnO nanowires. Because of their low power (140 W), low operating temperatures (90℃), easy fabrication (variable microwave sintering system), and low cost (90% cost reduction compared with gas condensation methods), high quality ZnO nanowires created with the rapid microwave heating process show great promise for use in flexible solar cells and flexible display devices.
机译:使用快速微波加热工艺成功地在玻璃基板上成功合成了取向良好的氧化锌(ZnO)纳米线阵列。 ZnO种子层是通过将前体溶液旋涂到基板上而产生的。在涂层中,将ZnO晶种层在100℃退火5分钟,以确保在空气,氮气和真空气氛下颗粒粘附到玻璃表面。随着直径大于30 nm的ZnO种子纳米粒子发展成为ZnO纳米线阵列,ZnO种子层的退火处理对于实现高质量的ZnO纳米线阵列至关重要。透射电子显微镜分析揭示了ZnO纳米线的单晶晶格。由于其低功率(140 W),低工作温度(90℃),易于制造(可变微波烧结系统)和低成本(与气体冷凝法相比,成本降低了90%),因此可以快速生成高质量的ZnO纳米线微波加热工艺显示出可用于柔性太阳能电池和柔性显示设备的巨大前景。

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