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METHOD OF STABILISING MESOSTRUCTURE OF MSM-41 TYPE SILICATE MATERIALS
METHOD OF STABILISING MESOSTRUCTURE OF MSM-41 TYPE SILICATE MATERIALS
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机译:稳定MSM-41型硅酸盐材料的细观结构的方法
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摘要
FIELD: chemistry.;SUBSTANCE: invention relates to synthesis of a MSM-41 type mesoporous material. The method involves stabilisation of the structure of the material during synthesis thereof, according to which the step for hydrothermal treatment in an autoclave is carried out while continuously stirring the reaction mixture at 105-135°C for 2-4 hours with molar ratio of reagents 1SiO2:0.6±0.2NH4Cl:1.6±0.2NH3:150H2O.;EFFECT: invention enables effective stabilisation of the mesostructure of MSM-41 material with low pressure of saturated vapour in the autoclave.;2 dwg, 2 tbl, 2 ex
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机译:发明领域本发明涉及MSM-41型中孔材料的合成。该方法包括在合成过程中稳定材料的结构,根据该方法,在高压釜中进行水热处理的步骤是在将反应混合物与试剂的摩尔比在105-135℃下连续搅拌2-4小时的同时进行的。 1SiO 2 Sub>:0.6±0.2NH 4 Sub> Cl:1.6±0.2NH 3 Sub>:150H 2 Sub> O .;效果:本发明能够在低压釜中饱和蒸汽的低压下有效稳定MSM-41材料的介孔结构。2dwg,2 tbl,2 ex
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