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Sample storage cell for X-ray microscope, X-ray microscope, and observation method of X-ray microscope image

机译:用于x射线显微镜的样品存储池,x射线显微镜以及x射线显微镜图像的观察方法

摘要

A sample support member (11) is provided with a metal film (11b) which emits characteristic X-rays in a wavelength range of 0.6 to 6.0 nm including the "water window" region when an electron beam strikes the metal film (11b) and which is provided on one main surface of a sample support film (11a) which is a silicon nitride film or a carbon film. Characteristic X-rays in the soft X-ray region are emitted with high efficiency (high intensity) from the metal film (11b) which the electron beam has struck. Since the high-intensity characteristic X-rays strike the sample (10), the SN ratio of the observation image is improved. Since th metal film (11b) has an effect of minimizing the range where electrons are diffused in the sample support film (11a), the damage to the sample is reduced. Further, since the acceleration voltage of the incident electron beam can be increased, the metal film (11b) has also an effect of improving the resolution.
机译:样品支撑构件(11)设置有金属膜(11b),当电子束撞击金属膜(11b)时,金属膜(11b)发出包括“水窗”区域在内的0.6至6.0nm波长范围内的特征X射线。它设置在样品支撑膜(11a)的一个主表面上,该样品支撑膜是氮化硅膜或碳膜。从电子束撞击的金属膜(11b)以高效率(高强度)发射软X射线区域中的特征X射线。由于高强度特征X射线撞击样品(10),因此观察图像的SN比提高。由于金属膜(11b)具有使电子在样品支撑膜(11a)中扩散的范围最小化的效果,所以减少了对样品的损害。此外,由于可以增加入射电子束的加速电压,因此金属膜(11b)也具有提高分辨率的效果。

著录项

  • 公开/公告号JP5317120B2

    专利类型

  • 公开/公告日2013-10-16

    原文格式PDF

  • 申请/专利权人 独立行政法人産業技術総合研究所;

    申请/专利号JP20090190871

  • 发明设计人 小椋 俊彦;

    申请日2009-08-20

  • 分类号G21K7;H01J37/20;G21K5/08;G21K3;G01N23/04;

  • 国家 JP

  • 入库时间 2022-08-21 16:58:54

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