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METHOD FOR PREPARING GRAPHENE ON SIC SUBSTRATE BASED ON ANNEALING WITH ASSISTANT METAL FILM

机译:基于辅助金属膜退火的SiC基体上石墨烯的制备方法

摘要

Provided are a method for preparing a graphene on SiC substrate based on annealing with assistant metal film and a double-layer graphene prepared thereby. The method comprises: normally cleaning the SiC substrate; introducing the cleaned SiC substrate into a quartz tube and heating it to 750-1150°C; inputting a CCl4 steam in the quartz tube with Ar gas and reacting with SiC to form a double-layer carbon film, wherein the reaction time is 20-100min; forming a metal film of 350-600nm on the SiC substrate via electron beam deposition; disposing the double-layer carbon film on the metal film and putting them all in Ar gas, annealing at the temperature of 900-1100°C for 10-30min to reconstruct the double-layer carbon film to form double-layer graphene; taking out of the metal film from the double-layer graphene sample wafer and obtaining a double-layer graphene.
机译:本发明提供了一种基于用辅助金属膜退火的方法在SiC衬底上制备石墨烯的方法以及由此制备的双层石墨烯。该方法包括:通常清洁SiC衬底;将清洗后的SiC衬底引入石英管中并加热至750-1150℃。向石英管中的氩气中输入CCl 4 蒸汽,与SiC反应形成双层碳膜,反应时间为20-100min。通过电子束沉积在SiC衬底上形成350-600nm的金属膜;将双层碳膜置于金属膜上,全部置于氩气中,在900-1100℃的温度下退火10-30min,以重构双层碳膜,形成双层石墨烯。从双层石墨烯样品晶片中取出金属膜,得到双层石墨烯。

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