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METHOD FOR PREPARING HYDROPHOBIC MONOLITH TYPE SILICA AEROGEL

机译:疏水性硅石气凝胶的制备方法

摘要

The present invention relates to a method for dipping monolith type silica aerogel synthesized in a alkylsilane solution which is a dipping solution using a alkoxide precursor and provides a method for preparing hydrophobic monolith type silica aerogel, wherein the method includes a step of making hydrophobic surface and inside of the monolith type silica wet gel. According to the present invention, hydrophobicity can be rapidly and economically given to monolith type silica aerogel in a simple way using a small amount of alkyl silane, the shrinkability of the hydrophobic monolith type silica aerogel is reduced, allows manufacture in a semi-transparent form, low thermal conductivity which is similar to the hydrophilic silica aerogel can be maintained, and application as a heat insulation plate is possible due to improved hydrophobicity and thermal insulation.;COPYRIGHT KIPO 2014;[Reference numerals] (AA) Monolith type wet gel producing step;(BB) Hydrogenating step using a dipping solution;(CC) Supercritical drying step;(DD) Hydrophobic silica aerogel
机译:本发明涉及将合成的整体式二氧化硅气凝胶浸渍在使用醇盐前体的浸渍溶液即烷基硅烷溶液中的方法,并提供制备疏水性整体式二氧化硅气凝胶的方法,其中该方法包括使疏水性表面和整体式硅胶湿凝胶内部。根据本发明,可以使用少量的烷基硅烷以简单的方式快速且经济地赋予整体式二氧化硅气凝胶疏水性,疏水性整体式二氧化硅气凝胶的收缩性降低,允许以半透明形式制造。 ,可以保持类似于亲水性二氧化硅气凝胶的低导热性,并且由于改善的疏水性和隔热性而可以用作隔热板。; COPYRIGHT KIPO 2014; [参考数字](AA)生产单块型湿凝胶步骤;(BB)使用浸渍溶液的氢化步骤;(CC)超临界干燥步骤;(DD)疏水性二氧化硅气凝胶

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