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Preparation method of hydrophobic monolith type silica aerogel

机译:疏水整体式二氧化硅气凝胶的制备方法

摘要

Provided is a method for preparing hydrophobic monolithic silica aerogel, comprising dipping monolithic wet silica gel obtained by using an alkoxide precursor into an alkylsilane solution as a dipping solution to perform hydrophobitization of the surface and inner part of the monolithic wet silica gel by a dipping process. The method is economical by virtue of the use of a small amount of alkylsilane compound and imparts hydrophobic property to monolithic silica aerogel simply in a cost efficient and time efficient manner. In addition, the method reduces shrinkage of hydrophobic monolithic silica aerogel, enables production of hydrophobic monolithic silica aerogel in a translucent form, and allows the hydrophobic monolithic silica aerogel to maintain low heat conductivity similar to the heat conductivity of hydrophilic silica aerogel. The hydrophobic monolithic silica aerogel may be used directly as a heat insulating panel by virtue of excellent hydrophobic property and heat insulating property.
机译:本发明提供一种疏水性整体硅胶气凝胶的制备方法,其包括将通过使用醇盐前体得到的整体式湿硅胶浸入烷基硅烷溶液中作为浸渍溶液,以通过浸渍工艺对整体式湿硅胶的表面和内部进行疏水化。 。该方法由于使用少量的烷基硅烷化合物是经济的,并且简单地以成本有效和时间有效的方式赋予整体二氧化硅气凝胶疏水性。另外,该方法减少了疏水性整体二氧化硅气凝胶的收缩,使得能够以半透明形式生产疏水性整体二氧化硅气凝胶,并且使疏水性整体二氧化硅气凝胶保持与亲水性二氧化硅气凝胶的热导率相似的低热导率。疏水性整体二氧化硅气凝胶由于优异的疏水性和绝热性而可以直接用作绝热板。

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