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Luminescence nanoparticle improving light emitting efficiency comprising zinc-silver-indium-sulfide and the method for manufacturing thereof by combichemistry
Luminescence nanoparticle improving light emitting efficiency comprising zinc-silver-indium-sulfide and the method for manufacturing thereof by combichemistry
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机译:包含锌-银-铟-硫的提高发光效率的发光纳米粒子及其组合化学制造方法
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invention - - - ((ZnxAgyInz)S2)(0.15 x 0.25, 0.35 y 0.45, 0.35 z 0.45, x + y + z = 1) is a composition of the nanoparticles and the method having the light emission. To this end, the present invention is a zinc-silver-stage constituting the library for the composition of the indium (step 1); Step introducing zinc precursor, silver precursor and the indium precursor and the vulcanizing agent according to the library configured in the above step 1 to each of the different reactor containing the solvent for preparing a metal precursor solution (step 2); Irradiating ultrasonic waves in the metal precursor solution in each reactor was prepared as described in Step 2 (Step 3); After ultrasonic irradiation in the stage 3 alcohol-based solvent, by addition of a hydrocarbon solvent, mixed solvents of the foregoing zinc-silver-indium-sulfide to precipitate the particles (step 4); Removing the supernatant and in the step 4 the particles are precipitated (step 5), and the supernatant was removed as described in Step 5 zinc-silver-indium-sulfide confirming the luminescence properties of the nanoparticles (step 6) ; provides a method comprising the. According to the present invention can be rapidly manufacturing a light emitting nanoparticles with various compositions, can be found by checking the light emission characteristics of the light emitting nano-particles is optimized to the desired composition. ;
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机译:发明--((Zn x Sub> Ag y Sub> In z Sub>)S 2 Sub>)(0.15 x 0.25,0.35 y 0.45,0.35 z 0.45,x + y + z = 1)是纳米粒子的组成和具有发光的方法。为此,本发明是构成铟的组成库的锌-银阶段(步骤1)。根据上述步骤1中配置的库,将锌前体,银前体以及铟前体和硫化剂分别引入到含有溶剂的不同反应器中,以制备金属前体溶液(步骤2);如步骤2(步骤3)所述,在各反应器的金属前驱体溶液中照射超声波。在阶段3的醇基溶剂中进行超声波照射后,通过加入烃溶剂,将前述锌-银-铟-硫化物的混合溶剂沉淀出来(步骤4);除去上清液,并在步骤4中沉淀出颗粒(步骤5),然后按照步骤5中所述的方法除去上清液,从而确认了纳米银的发光特性(步骤6);提供一种包括该方法的方法。根据本发明,可以快速制造具有各种组成的发光纳米粒子,可以通过检查将发光纳米粒子的发光特性优化至所需组成来发现。 ;
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