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METHOD FOR DETERMINING thiacloprid in biological objects using high performance liquid chromatography

机译:高效液相色谱法测定生物对象中噻虫啉的方法

摘要

A method for determining thiacloprid in biological objects using high performance liquid chromatography, comprising sample selection, extraction, filtration, sodium dehydration sulfate anhydrous, evaporation, introduction of dissolved dry residue into the chromatograph, processing the analysis results, characterized in that the sample take a sample of an organ or tissue animals weighing 50 to 200 mg, extraction was performed with acetone, dissolved dry residue is taken up in the liquid chromatograph "Chromos - LC 301" with spectrophotometer detector matic and UVV 104M column Diasfer - 110C - 16 (150 × 4) mm with a particle size of sorbent 5 m, as the eluent a mixture of acetonitrile - water 30:70.
机译:一种使用高效液相色谱法测定生物对象中噻虫啉的方法,包括样品的选择,提取,过滤,无水硫酸钠脱水,蒸发,将溶解的干燥残留物引入色谱仪,处理分析结果,其特征在于样品取称重50至200 mg的器官或组织动物的样品,用丙酮进行萃取,将溶解的干燥残留物吸收在液相色谱仪“ Chromos-LC 301”中,并使用分光光度计检测器matic和UVV 104M色谱柱Diasfer-110C-16(150 ×4)mm,吸附剂的粒径为5 m,乙腈-水30:70的混合物作为洗脱液。

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