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HIGH-DENSITY HIGH-RIGIDITY GRAPHENE POROUS CARBON MATERIAL AND PREPARATION METHOD AND APPLICATION THEREOF

机译:高密度高刚性石墨烯多孔碳材料及其制备方法与应用

摘要

The present disclosure provides a graphene-based porous carbon material with high-density and high-hardness, a method for making the same, and applications thereof. The method includes following steps: step 1, forming an original sol by adding a graphene-based component or a mixture of a graphene-based component and an auxiliary component in a solvent and dispersing the graphene-based component to obtain the original sol for preparing the graphene-based porous carbon material; step 2, preparing a graphene-based gel by placing the original sol prepared in step 1 in a reacting container and heating the original sol to a temperature of about 20°C to about 500°C for about 0.1 hours to about 100 hours; step 3, preparation of the graphene-based porous carbon material with high-density and high-hardness: after drying the gel at a temperature of about 0°C to about 200°C, heating the gel in an oxygen-deficient atmosphere and a temperature of about 100°C to about 3600°C for about 0.1 hours to about 100 hours, or/and activating the gel at a temperature of about 200°C to about 2000°C for about 0.1 hours to about 50 hours. Compared with the prior art, the prepared graphene-based material has the advantage of high density, high hardness, abundant pores, large specific surface area and stable pore structure.
机译:本公开提供了一种具有高密度和高硬度的石墨烯基多孔碳材料,其制备方法及其应用。该方法包括以下步骤:步骤1,通过在溶剂中加入石墨烯基组分或石墨烯基组分与辅助组分的混合物,形成原始溶胶,并将石墨烯基组分分散,得到用于制备的原始溶胶。石墨烯基多孔碳材料;步骤2,通过将步骤1中制备的原始溶胶置于反应容器中,并将原始溶胶加热至约20℃至约500℃的温度约0.1小时至约100小时,从而制备石墨烯基凝胶。步骤3,制备高密度高硬度的石墨烯基多孔碳材料:在约0℃至约200℃的温度下干燥凝胶后,在缺氧气氛中加热凝胶。在约100℃至约3600℃的温度下进行约0.1小时至约100小时,或/和在约200℃至约2000℃的温度下活化凝胶约0.1小时至约50小时。与现有技术相比,所制备的石墨烯基材料具有密度高,硬度高,孔丰富,比表面积大和孔结构稳定的优点。

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