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HIGH-DENSITY HIGH-RIGIDITY GRAPHENE POROUS CARBON MATERIAL AND PREPARATION METHOD AND APPLICATION THEREOF

机译:高密度高刚性石墨烯多孔碳材料及其制备方法与应用

摘要

Disclosed are a high-density high-rigidity graphene porous carbon material and a preparation method and application thereof. The method comprises the following steps: 1. original colloidal sol preparation: adding a graphene-based component or a mixture of a graphene-based component and auxiliary components into a solvent for dispersion to obtain an original colloidal sol for preparing the graphene porous carbon material; 2. graphene-based gel preparation: placing the original colloidal sol prepared in Step 1 into a reaction container, reacting for 0.1-100 hours at a temperature of 20-500°C to obtain the graphene-based gel; and 3: high-density high-rigidity graphene porous carbon material preparation: drying the graphene-based gel at a temperature of 0-200°C, increasing the temperature to 100-3600°C in anoxic atmosphere for conducting thermal treatment for 0.1-100 hours, and/or reacting for 0.1-50 hours at a temperature of 200-2000°C by adopting an activation reaction method. Compared with the prior art, the prepared graphene-based material has the advantages of high density, high rigidity, abundant pores, large specific surface area and stable pore structure.
机译:本发明公开了一种高密度高刚性石墨烯多孔碳材料及其制备方法和应用。该方法包括以下步骤:1.原始胶体溶胶的制备:将石墨烯基组分或石墨烯基组分与辅助组分的混合物加入到溶剂中进行分散,以获得用于制备石墨烯多孔碳材料的原始胶体溶胶。 ; 2.石墨烯基凝胶制剂:将步骤1中制备的原始胶体溶胶放入反应容器中,在20-500℃的温度下反应0.1-100小时,得到石墨烯基凝胶。 3:高密度高刚度石墨烯多孔碳材料的制备:将石墨烯基凝胶在0-200°C的温度下干燥,在缺氧气氛中将温度升至100-3600°C进行0.1- 100小时,和/或采用活化反应法,在200-2000℃的温度下反应0.1-50小时。与现有技术相比,所制备的石墨烯基材料具有密度高,刚性高,孔丰富,比表面积大,孔结构稳定的优点。

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