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METHOD FOR ESTABLISHING SHENQI FUZHENG INJECTION FINGERPRINT SPECTRUM
METHOD FOR ESTABLISHING SHENQI FUZHENG INJECTION FINGERPRINT SPECTRUM
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机译：建立申岐扶正注射指纹图谱的方法
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摘要
A method for establishing a Shenqi Fuzheng injection fingerprint spectrum, comprising: employing an ultra-high voltage liquid chromatography mass spectrometer to test the Shenqi Fuzheng injection, the chromatography conditions including: chromatographic column: Agilent Zorbax Eclipse Plus C18, 2.1 mm x 100 mm, 1.8 µm; mobile phase: mobile phase A is 0.1 % formic acid aqueous solution, and mobile phase B is 0.1% formic acid acetonitrile solution; employing gradient elution procedure as follows: 0-0.5 min, 95% of mobile phase A, and 5% of mobile phase B; 0.5-10 min, 95%-75% of mobile phase A, and 5%-25% of mobile phase B; 10-15 min, 75%-45% of mobile phase A, and 25%-55% of mobile phase B; 15-18 min, 45%-0% of mobile phase A, and 55%-100% of mobile phase B; and 18-20 min, 0% of mobile phase A, and 100% of mobile phase B.
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机译：一种建立参芪扶正注射液指纹图谱的方法，包括：采用超高压液相色谱质谱仪测试参芪扶正注射液，色谱条件包括：色谱柱：Agilent Zorbax Eclipse Plus C18，2.1 mm x 100 mm， 1.8微米;流动相：流动相A为0.1％甲酸水溶液，流动相B为0.1％甲酸乙腈溶液。采用以下梯度洗脱程序：0-0.5分钟，流动相A的95％，流动相B的5％。 0.5-10分钟，流动相A的95％-75％，流动相B的5％-25％; 10-15分钟，流动相A的75％-45％，流动相B的25％-55％; 15-18分钟，流动相A的45％-0％，流动相B的55％-100％;和18-20分钟，分别为流动相A的0％和流动相B的100％。
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