首页> 外国专利> PREPARATION METHOD OF POLYVINYLIDENE FLUORIDE NANOPARTICLE AND POLYVINYLIDENE FLUORIDE NANOPARTICLE PREPARED THEREBY

PREPARATION METHOD OF POLYVINYLIDENE FLUORIDE NANOPARTICLE AND POLYVINYLIDENE FLUORIDE NANOPARTICLE PREPARED THEREBY

机译:聚偏氟乙烯纳米颗粒的制备方法及其制备的聚偏氟乙烯纳米颗粒

摘要

The present invention relates to a polyvinylidene fluoride (PVDF) nanoparticle preparation method. The method includes the steps of: preparing a mixed solution by mixing a radical initiator, a surfactant, and distilled water in an reaction vessel (step 1); and making the reaction vessel storing the mixed solution prepared in the step 1 reach the reaction temperature of 60-90°C and the reaction pressure of 10-100 bar and stirring the mixed solution at the speed of 100-1,000 rpm, and adding vinylidene fluoride (VDF) at the rate of 0.5-2 g/min to initiate the reaction thereof (step 2). According to the present invention, the PVDF nanoparticle preparation method can adjust the molecular weight of the PVDF nanoparticles by adjusting the reaction conditions. Accordingly, the PVDF nanoparticles prepared by the method can have the properties satisfying the requirements of various fields.;COPYRIGHT KIPO 2015
机译:本发明涉及聚偏氟乙烯(PVDF)纳米颗粒的制备方法。该方法包括以下步骤:通过在反应容器中混合自由基引发剂,表面活性剂和蒸馏水来制备混合溶液(步骤1);使储存有步骤1中制备的混合溶液的反应容器达到反应温度60-90℃和反应压力10-100bar,并以100-1,000rpm的速度搅拌混合溶液,并加入亚乙烯基氟化物(VDF)以0.5-2 g / min的速率引发反应(步骤2)。根据本发明,PVDF纳米颗粒的制备方法可以通过调节反应条件来调节PVDF纳米颗粒的分子量。因此,通过该方法制备的PVDF纳米颗粒可以具有满足各个领域要求的性能。; COPYRIGHT KIPO 2015

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