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METHOD OF PRODUCING ULTRAFINE POWDER OF SILVER AND SILVER ULTRAFINE POWDER OBTAINED USING SAID METHOD

机译:制备银超细粉的方法及采用suid方法制得的银超细粉

摘要

FIELD: medicine.;SUBSTANCE: invention relates to methods for obtaining powder material containing microparticles, and can be used in medicine as a bactericidal material, in chemistry for purification of drinking water; in production of catalysts; in chemical industry for protective coating of pipeline walls; in the chemical current sources. Method of producing ultrafine silver powder includes treatment of water solution of silver nitrate with reducing agent. As a reducing agent the aqueous solution of thiocarbonic acid (thiourea) and ammonium hydroxide is used taken in the following ratio: silver nitrate:thiocarbonic acid diamide (thiourea):ammonium hydroxide = 1:5÷10:0.01÷0.8. Obtained ultradisperse silver powder contains modified particles of star-like shape, having from 32 to 56 pyramidal and wedge-like beams with length of 40-50 microns with average size of the core 5-6 microns, the density of powder is equal to 0.4-0.8 g/cm3.;EFFECT: technical result consists in obtaining of pure metal particles of silver, characterised with modified structure of surface morphology, simple efficient method using safe and ecologically pure substances.;2 cl, 2 dwg, 2 ex
机译:含有微粒的粉末材料的制备方法技术领域本发明涉及获得含有微粒的粉末材料的方法,并且可以在医学上用作饮用水净化化学中的杀菌材料。在催化剂生产中;在化学工业中用于管道壁的防护涂层;在化学电流源中。制备超细银粉的方法包括用还原剂处理硝酸银的水溶液。作为还原剂,以以下比例使用硫代碳酸(硫脲)和氢氧化铵的水溶液:硝酸银:硫代碳酸二酰胺(硫脲):氢氧化铵= 1:5÷10:0.01÷0.8。获得的超分散银粉包含星形的改性颗粒,具有32至56个金字塔形和楔形光束,其长度为40-50微米,芯的平均尺寸为5-6微米,粉末的密度等于0.4 -0.8 g / cm 3 .;效果:技术成果在于获得纯净的银金属颗粒,其特征在于表面形态结构发生改变,使用安全且生态纯净的物质的简便有效方法。; 2 cl ,2 dwg,2前

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