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SYSTEM AND METHOD FOR THE SOLVENT EXTRACTION PROCESS mother liquor PURE

机译:溶剂萃取过程母液纯的系统和方法

摘要

1. A process for extracting pure residual mother liquor (CHOMR), resulting in obtaining pure terephthalic acid (chTFK) comprising: combining CHOMR with a solution containing an organic entrainer to produce a mixture wherein CHOMR temperature of at least about 20 ° C less than the azeotropic temperature of the solution comprising the organic entrainer, separating the mixture into an organic stream containing residual aromatic carboxylic acid and the aqueous stream, heating the organic stream pU it heat exchange with the effluent from the distillation column, heated to form the organic stream, heating the aqueous stream by heat exchange with the effluent from the regeneration column to form a heated water stream, supplying the heated organic stream to a distillation column; and supply line at least a portion of the heated water stream in the regeneration kolonnu.2. The method of claim. 1, characterized in that it further comprises feeding a second part of the heated water stream into the distillation kolonnu.3. The method of claim. 1, characterized in that the organic entrainer selected from the group consisting of toluene, xylene, ethylbenzene, methylbutyl ketone, chlorobenzene, etilamilovogo ether, butyl formate, n-propyl, isopropyl, n-butyl acetate, isobutyl acetate, amyl acetate, methyl acetate, n -butilpropionata, izobutilpropionata, propanol, water and smesey.4. The method of claim. 1, characterized in that CHOMR temperature of at least about 25 ° C lower than the azeotropic temperature of the solution containing the organic azeotropoobrazovatel.5. The method of claim. 1, characterized
机译:1.一种提取纯残留母液(CHOMR),从而获得纯对苯二甲酸(chTFK)的方法,该方法包括:将CHOMR与包含有机夹带剂的溶液合并以产生混合物,其中CHOMR温度至少低于约20℃。包含有机夹带剂的溶液的共沸温度,将混合物分离为含有残留芳族羧酸的有机物流和水物流,加热有机物流,使其与蒸馏塔的流出物进行热交换,加热以形成有机物流通过与来自再生塔的流出物进行热交换来加热水流以形成加热的水流,将加热的有机流供应至蒸馏塔;并供给至少一部分再生中的热水流。2。权利要求的方法。 1,其特征在于,它还包括将第二部分热水流进料到蒸馏kolonnu.3中。权利要求的方法。 1,特征在于有机夹带剂选自甲苯,二甲苯,乙苯,甲基丁基酮,氯苯,戊二醇醚,甲酸丁酯,正丙基,异丙基,乙酸正丁酯,乙酸异丁酯,乙酸戊酯,乙酸甲酯,n-butilpropionata,izobutilpropionata,丙醇,水和smesey。4。权利要求的方法。 1,其特征在于,CHOMR温度至少比含有有机共沸杂唑烷的溶液的共沸温度低约25℃。5。权利要求的方法。 1,特点

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