首页> 外国专利> METHOD FOR SEPARATING N,N,N'-TRIMETHYLBISAMINOETHYLETHER AND/OR N,N-DIMETHYLBISAMINOETHYLETHER FROM A MIXTURE

METHOD FOR SEPARATING N,N,N'-TRIMETHYLBISAMINOETHYLETHER AND/OR N,N-DIMETHYLBISAMINOETHYLETHER FROM A MIXTURE

机译:从混合物中分离N,N,N'-三甲基双亚氨基乙基醚和/或N,N-二甲基双亚氨基乙基醚的方法

摘要

The present invention relates to a method for separating N,N,N'-trimethylbisaminoethylether and/or N,N-dimethylbisaminoethylether, from a mixture A comprising N,N,N'-trimethylbisaminoethylether, and N,N-dimethylbisaminoethylether, wherein said method comprises the steps of: (a) contacting said mixture A with an acylating agent, to form a mixture B comprising the amides of N,N,N'-trimethylbisaminoethylether and of N,N-dimethylbisaminoethylether, respectively; and (b1) separating the amide of N,N,N'-trimethylbisaminoethylether from mixture B; and (c1) recovering N,N,N'-trimethylbisaminoethylether from its amide by means of a transamidation reaction; and/or (b2) separating the amide of N,N-dimethylbisaminoethylether from mixture B; and (c2) recovering N,N-dimethylbisaminoethylether from its amide by means of a transamidation reaction.
机译:本发明涉及从包含N,N,N'-三甲基双氨基乙基醚和N,N-二甲基双氨基乙基醚的混合物A中分离N,N,N'-三甲基双氨基乙基醚和/或N,N-二甲基双氨基乙基醚的方法,其中所述方法包括以下步骤:(a)使所述混合物A与酰化剂接触,以形成分别包含N,N,N′-三甲基双氨基乙基醚和N,N-二甲基二氨基乙基醚的酰胺的混合物B;和(b1)从混合物B中分离出N,N,N'-三甲基双氨基乙基醚的酰胺; (c1)通过酰胺基转移反应从其酰胺中回收N,N,N'-三甲基双氨基乙基醚;和/或(b2)从混合物B中分离出N,N-二甲基双氨基乙基醚的酰胺; (c2)通过酰胺基转移反应从其酰胺中回收N,N-二甲基双氨基乙基醚。

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