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Method for preparing double-sealed-end glycol ether
Method for preparing double-sealed-end glycol ether
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机译:一种双封端乙二醇醚的制备方法
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摘要
Disclosed is a method for preparing a double end capped glycol ether, the method comprising: introducing into a reactor a raw material comprising a glycol monoether and a monohydric alcohol ether, and enabling the raw material to contact and react with an acidic molecular sieve catalyst to generate a double end capped glycol ether, a reaction temperature being 50-300° C., a reaction pressure being 0.1-15 MPa, a WHSV of the glycol monoether in the raw material being 0.01-15.0 h−1 , and a mole ratio of the monohydric alcohol ether to the glycol monoether in the raw material being 1-100:1. The method of the present invention enables a long single-pass lifespan of the catalyst and repeated regeneration, has a high yield and selectivity of a target product, low energy consumption during separation of the product, a high economic value of a by-product, and is flexible in production scale and application.
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机译:公开了一种制备双末端封端的二醇醚的方法,该方法包括:将包含二醇单醚和一元醇醚的原料引入反应器中,并使该原料与酸性分子筛催化剂接触并反应,以使之生成双封端的乙二醇醚,反应温度为50-300°C,反应压力为0.1-15 MPa,原料中的二醇单醚的WHSV为0.01-15.0 h -1 Sup>,并且原料中一元醇醚与二醇单醚的摩尔比为1-100:1。本发明的方法能够使催化剂具有长的单程寿命并重复再生,具有目标产物的高产率和选择性,产物分离过程中的能量消耗低,副产物的经济价值高,生产规模和应用灵活。
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