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Preparing method of transition metal-nitrogen doped porous carbon catalyst

机译:过渡金属氮掺杂多孔碳催化剂的制备方法

摘要

The present invention relates to a process for preparing a slurry by mixing a precursor containing carbon, a transition metal and nitrogen, a silica template and a solvent (first step); Heating the slurry to evaporate the solvent to form a powdery composite (second step); Carbonizing the composite by heating under an inert gas, and cooling the composite to form crystalline carbon (the third step); And a step of washing the crystalline carbon with an acid to form a porous carbon catalyst (fourth step), and a porous carbon catalyst prepared by the method. The porous carbon catalyst doped with the transition metal and nitrogen does not use an expensive platinum catalyst and is easily produced in a one-pot process by using a precursor containing both carbon, transition metal and nitrogen, The carbon catalyst of a thin thickness can be formed by using the precursor of the fuel cell, thereby increasing the economical efficiency of the fuel cell manufacturing process and greatly increasing the reduction characteristic of the cathode electrode of the fuel cell.
机译:本发明涉及通过混合含有碳,过渡金属和氮的前体,二氧化硅模板和溶剂来制备浆料的方法(第一步)。加热浆液以蒸发溶剂以形成粉末状复合材料(第二步);通过在惰性气体下加热将复合材料碳化,然后冷却复合材料以形成结晶碳(第三步);以及用酸洗涤结晶碳以形成多孔碳催化剂的步骤(第四步骤),以及通过该方法制备的多孔碳催化剂。掺杂有过渡金属和氮的多孔碳催化剂不使用昂贵的铂催化剂,并且通过使用同时包含碳,过渡金属和氮的前体,可以在一锅法中容易地生产,可以形成厚度薄的碳催化剂。通过使用燃料电池的前体形成的燃料电池,可以提高燃料电池制造工艺的经济效率,并且可以大大提高燃料电池的阴极的还原特性。

著录项

  • 公开/公告号KR101808910B1

    专利类型

  • 公开/公告日2018-01-19

    原文格式PDF

  • 申请/专利权人 숭실대학교산학협력단;

    申请/专利号KR20150117398

  • 发明设计人 박경원;이슬;곽다희;이진연;

    申请日2015-08-20

  • 分类号B01J37;B01J27/24;B01J37/08;H01M4/90;

  • 国家 KR

  • 入库时间 2022-08-21 12:38:46

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