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METHOD FOR OBTAINING PLASTICISERS

机译:求助者的方法

摘要

FIELD: technological processes.;SUBSTANCE: invention relates to a process for obtaining a plasticizer. This method comprises mixing the raw material with a solvent, selective purification and subsequent distillation of the solvent from the raffinate and extract solutions. Said method is characterized in that a distillate extract of the fraction 450–550 °C, obtained as a result of selective purification of petroleum oil fraction with a boiling point of 450–550 °C, or an extract of a mixture of the distillate fraction 450–550 °C, obtained by distilling oil with a boiling point of 450–550 °C, and deasphalted product obtained in the process of deasphalting tar with propane. As a solvent, a solution containing, by weight, %: water 2.0, N-methylpyrrolidone is the rest, the mass ratio of raw materials: solvent is set equal to 1:0.8–1.2, the resulting mixture is stirred for 25–30 minutes, and selective purification of raw materials is carried out by purification steps at temperatures 35 °C, 40 °C, 45 °C or 40 °C, 45 °C, 50 °C, setting the settling time at each purification stage of 25–30 minutes.;EFFECT: increased efficiency and selectivity of the selective purification process by reducing the total raw material: solvent ratio to produce a plasticizer that meets the requirements of Directive 2005/69/EC.;1 cl, 6 ex, 1 tbl
机译:增塑剂的制备方法技术领域本发明涉及一种增塑剂的制备方法。该方法包括将原料与溶剂混合,选择性纯化以及随后从萃余液和萃取液中蒸馏出溶剂。所述方法的特征在于,通过选择性地纯化沸点为450-550℃的石油馏分得到的馏分450-550℃的馏出物提取物,或馏分混合物的提取物。通过蒸馏沸点为450-550°C的油获得的450-550°C的温度,以及在用丙烷对沥青进行脱沥青的过程中获得的脱沥青产品。作为溶剂,剩下的是重量百分比为:水2.0,N-甲基吡咯烷酮的溶液,原料:溶剂的质量比设置为等于1:0.8-1.2,将所得混合物搅拌25-30分钟,然后在35°C,40°C,45°C或40°C,45°C,50°C的温度下通过纯化步骤进行原料的选择性纯化,将每个纯化阶段的沉降时间设置为25 –30分钟。;效果:通过减少原料,溶剂的总比来生产符合指令2005/69 / EC要求的增塑剂,从而提高了选择性纯化工艺的效率和选择性。1cl,6 ex,1 tbl

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