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Cobalt Ferrite Nanoparticles Fabricated via Co-precipitation in Air: Overview of Size Control and Magnetic Properties

机译:通过空气中共沉淀制备的钴铁氧体纳米粒子:尺寸控制和磁性的概述

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摘要

Cobalt Ferrite has important, size-dependent magnetic properties. Consequently, an overview of particle size is important. Co-precipitation in air was the fabrication method used because it is comparatively simple and safe. The effects of three different reaction times including 1, 2, 3 hour(s) on particle size were compared. Also, the effectiveness of three different capping agents (Oleic Acid, Polyvinylpyrollidone (PVP), and Trisodium Citrate) in reducing aggregation and correspondingly particle size were examined. Using Welch’s analysis of variance (ANOVA) and the relevant post hoc tests, there was no significant difference (p=0.05) between reaction times of 1 hour and 2 hours, but there was a significant difference between reaction times of 2 hours and 3 hours. Potentially, because of increased coarsening for the 3 hour reaction time. PVP and Oleic Acid were shown to be effective in reducing aggregation; however, Citrate was not effective. Possibly, the synthesis procedure was inadequate.
机译:铁氧体钴具有重要的,尺寸依赖性的磁性。因此,粒度概述很重要。空气中的共沉淀是使用的制造方法,因为它相对简单且安全。比较了三个不同的反应时间(包括1、2、3小时)对粒径的影响。同样,检查了三种不同的封端剂(油酸,聚乙烯吡咯烷酮(PVP)和柠檬酸三钠)在减少聚集和相应地减小粒径方面的有效性。使用Welch方差分析(ANOVA)和相关的事后检验,1小时和2小时的反应时间之间无显着差异(p = 0.05),但2小时和3小时的反应时间之间有显着差异。可能是由于3小时反应时间的粗化程度增加。 PVP和油酸可有效减少聚集;但是,柠檬酸盐无效。可能是合成程序不充分。

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    Toledo Dennis;

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  • 年度 2015
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