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On the Anodization Trimming of Ti-Si0_2 Cermet Thin Film Resistors

机译:Ti-Si0_2金属陶瓷薄膜电阻的阳极氧化修整

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摘要

The trimming of the resistance of thin film resistors has been carried out by cutting their size with mechanical cutter or laser beam. However, the cutting method generally introduces micro-cracking into the thin films. The cermet thin films consisting of Si0_2 and metal are deposited more thickl compared with metal thin film resistors, but are rather weak against mechanical and thermal shock. Therefore, we have investigated the trimming by changing the film thckiness by anodic oxidation for cermet thin film resistors. The Ti-Si0_2 cermet thin films were anodized for 30 minutes at several different anodizing voltages using filter papers, which were wetted with Dimethyl Sulfoxide-Phosphoric Acid (20%)solution, and sandwiched between the film and top cathode electrode. The films showed a wide resistance change by anodization, but the anodized film resistors were not so stable as expected. By an anodization with the voltage lower than 15 volts, the trimming of less than 5% is possible and reproducible. The heat-treatment in air after anodization developed markedly the stability of resistance. The cermet thin films, heat-treated at 300℃ for 3 hrs. in air after anodization at 50 volts, showed fairly good stability and a resistance change of less than 1% by a 1000-hour stability test at 125℃ in air. The films sputtered from a composite target with a 16% SiO_2 area ratio provided the most stable cermet thin film resistors. It was found that the anodization?heat-treatment combination is the most valuable trimming method in order to realize the exact and stable Ti-SiO_2 cermet thin film resistors.
机译:通过使用机械切割器或激光束切割薄膜电阻器的尺寸来进行薄膜电阻器的微调。然而,切割方法通常将微裂纹引入薄膜中。与金属薄膜电阻器相比,由SiO 2和金属组成的金属陶瓷薄膜沉积得更厚,但抗机械冲击和热冲击的能力较弱。因此,我们研究了通过阳极氧化改变金属陶瓷薄膜电阻器的膜厚的修整方法。用滤纸在几种不同的阳极氧化电压下对Ti-SiO 2金属陶瓷薄膜进行阳极氧化30分钟,然后用二甲基亚砜-磷酸(20%)溶液润湿并夹在薄膜和顶部阴极之间。这些膜通过阳极氧化显示出宽广的电阻变化,但是阳极氧化膜电阻并不像预期的那样稳定。通过在低于15伏的电压下进行阳极氧化,可将修整度降低到5%以下,并且可重复进行。阳极氧化后在空气中进行热处理显着提高了电阻的稳定性。金属陶瓷薄膜在300℃热处理3小时。在空气中经过50伏阳极氧化后,在125伏的条件下进行1000小时的稳定性测试,显示出相当好的稳定性,并且电阻变化小于1%。从具有16%SiO_2面积比的复合靶溅射得到的薄膜提供了最稳定的金属陶瓷薄膜电阻器。为了实现精确而稳定的Ti-SiO_2金属陶瓷薄膜电阻器,阳极氧化热处理组合是最有价值的修整方法。

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