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Characteristics of Nanocrystalline Zirconia Powder in the ZrO2- Y2O3-CeO2-Al2O3 system with 0.1wt. СоО

机译:ZrO2- Y2O3-CeO2-Al2O3体系中0.1wt。%СоО的纳米晶氧化锆粉的特性

摘要

Matrix (mol%) 95ZrO2-3Y2O3-2CeO2 was produced by hydrothermal synthesis from a mixture of previously precipitated hydroxides. -Al2O3 and Co(NO3)3 were added by mechanical mixing. The properties of nanocrystalline powders with a complex chemical composition (wt.) [90 (ZrO2-CeO2-Y2O3)-10Al2O3]-(0,1Al2O3-0,1CoO) after heat treatment in the temperature range from 400 to 1300 °C were investigated by XRD phase analysis and BET measurements. During heat treatment powders retained in nanocrystallite state (primary particle size of the zirconia solid solution varies from 14 to 83 nm), and its specific surface area decreases from 99,7 m2/g to 1.51 m2/g.When you are citing the document, use the following link http://essuir.sumdu.edu.ua/handle/123456789/35263
机译:通过水热合成由先前沉淀的氢氧化物的混合物产生基质(mol%)95ZrO2-3Y2O3-2CeO2。通过机械混合添加-Al 2 O 3和Co(NO 3)3。在400至1300°C的温度范围内进行热处理后,具有复杂化学成分(wt。)[90(ZrO2-CeO2-Y2O3)-10Al2O3]-(0,1Al2O3-0,1CoO)的纳米晶体粉末的性能为通过XRD相分析和BET测量进行了研究。在热处理过程中,以纳米微晶状态保留的粉末(氧化锆固溶体的初级粒径从14到83 nm不等),其比表面积从99.7 m2 / g降低到1.51 m2 / g。 ,请使用以下链接http://essuir.sumdu.edu.ua/handle/123456789/35263

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